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Report Number: 43342 QC Report : Matrix Spike] Matrix Spike Duplicate Date : 4/2612005 Project Name : Sanchez Property Project Number: Duplicate Spiked Duplicate Spiked Spiked Sample Relative Spike Spiked Spiked Sample Sample Relative Percent Percent Spiked Sample Spike Dup. Sample Sample Analysis Date Percent Percent Percent Recov. Diff. Parameter Sample Value Level Level Value Value Units Method Analyzed Recov. Recov. Diff. Limit Limit Benzene 43352-01 <0.50 40.0 40.0 42.5 41.1 ug/L EPA 8260B 4121105 106 103 3.22 70-130 25 Toluene 43352-01 1.1 40.0 40.0 38.7 37.3 ug/L EPA 8260E 4/21105 94.0 90.6 3.69 70-130 25 Tert-Butanol 43352-01 <5.0 200 200 212 197 ug/L EPA 8260B 4/21105 106 98.6 7.28 70-130 25 Methyl-t-Butyl Ether 43352-01 <0.50 40.0 40.0 33.4 34.0 ug/L EPA 8260B 4121105 83.5 85.0 1.79 70-130 25 Benzene 43342-06 64 40.0 40.0 108 107 ug/L EPA 8260E 4122105 111 108 2.56 70-130 25 Toluene 43342-06 3.6 40.0 40.0 43.5 43.4 ug/L EPA 8260E 4122/05 99.8 99.5 0.224 70-130 25 Tert-Butanol 43342-06 10 200 200 213 206 ug/L EPA 8260B 4122105 102 97.9 3.68 70-130 25 Methyl-t-Butyl Ether 43342-06 29 40.0 40.0 65.7 66.1 ug/L. EPA 8260E 4122105 91.9 93.0 1.17 70-130 25 Benzene 43342-08 <0.50 40.0 40.0 37.4 36.5 ug/L EPA 8260B 4123105 93.4 91.4 2.20 70-130 25 Toluene 43342.08 <0.50 40.0 40.0 37.8 37.2 ug/L. EPA 8260E 4/23105 94.6 93.0 1.60 70-130 25 Tert-Butanol 43342-08 <5.0 200 200 197 197 ug/L EPA 82608 4123105 98.4 98.7 0.344 70-130 25 Methyl-t-Butyl Ether 43342-08 <0.50 40.0 40.0 37.0 36.7 ug/L EPA 8260E 4123105 92.5 91.8 0.799 70-130 25 Benzene 43342-12 <0.50 40.0 40.0 42.3 41.8 ug/L EPA 8260B 4122105 106 104 1.23 70-130 25 Toluene 43342-12 <0.50 40.0 40.0 42.3 41.8 ug/L EPA 82608 4122/05 106 104 1.36 70-130 25 Tert-Butanol 43342-12 <5.0 200 200 209 204 ug/L EPA 8260B 4122105 104 102 2.28 70-130 25 Methyl-t-Butyl Ether43342-12 <0.50 40.0 40.0 431 43.0 ug/L EPA 8260B 4122105 108 107 0.277 70-130 25 Benzene 43355-19 <0.50 40.0 40.0 41.2 40.1 ug/L EPA 8260B 4123105 103 100 2.78 70-130 25 Toluene 43355-19 <0.50 40.0 40.0 41.6 40.7 ug/L EPA 82606 4123105 104 102 2.16 70-130 25 Approved By: Jo iff KIFF ANALYTICAL, LLC 2795 2nd St, Suite 300 Davis, CA 95616 530-297-4800