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Sequoia 680 Chesapeake Cinve Reduiocd City,CA 95063 (6S0) 364-9600 FAX(650)364-9233 <br /> 505N,Wiget Lane Walmt Creek,CA 91598 (510) 988-9600 FAX(510)988-9671 <br /> Analytical 919 St6ker Avenue,Suite a Sxramento,CA 95834 (916) 921-9600 FAX(91,$)92i-0100 <br /> Blaine Tech Services Inc. Client Project lb: Shell Stockton /970805-S1 - <br /> 1680 Rogers Avenue MatrDc: Liquid <br /> San Jose, CA 95112 <br /> Attention Fran Thie Work Order#: 9708341-01,02 Reponed- Aug 13, 1997: <br /> QUALITY CONTROL DATA REPORT <br /> Analyte: MT8E <br /> OC Batch#: MS0812971ATBEH6A <br /> Analy. Method: EPA 8260 <br /> Prep. Method: N.A. <br /> Analyst: M.Williams <br /> MS/MSD#: 97osis&o1 <br /> Sample Conc: N.O. <br /> Prepared Date: 8/12/97 <br /> Analyzed Date: 8/12/97 <br /> Instrument I.D.#: F16 <br /> Conc. Spiked: 50yg/L <br /> Resuh: 52 <br /> MS%Recovery: 104 <br /> Dup. Result: 52 <br /> MSD% Recov.: 104 <br /> RPD: 0.0 <br /> RPD Lima: 0-25 <br /> i a 4;,1p�.T <br /> LCS#: VMBM1297 <br /> Prepared Date: 8;12/97 <br /> Analyzed Date: 8/12/97 <br /> Instrument I.D.#: FI6 <br /> Conc. Spiked: 50pg/L <br /> LCS Result: 51 <br /> LCS%Recov.: 102 <br /> 60-140 <br /> LCS 70-130 <br /> Control Limits <br /> Please Note <br /> The LCS is a control sample of known,interferent-free matrix that is analysed using the Same raagants, <br /> SEQUOIA A LYTICAL preparation,and analytical memods employed for samples. The matux spike is an aliquot of sample <br /> fortified with known quan6tlas of specific compounds and subjected to the entire analytical procedure. 8 <br /> the recovery of anaMtes from the matrix spike does not fall within specified control limits due to matrix <br /> he a Finterference,the LCS recovery is to be used to validate the batch. <br /> lynn -- <br /> Project Manager MS=Matrix Spike,MSD=MS Duplicate,RPD=Relative%Difference 9708341 BLA <4> <br /> t 1 d kaod� Wd8D'Z L661-V l-8 <br />