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COULAB CORE LABORATORIES S U R R 0 G A T E R E C 0 V E R I E S R E P O R T Job Number 990877 Report Date 05/31/1999 CUSTOMER IT Group PROJECT, Southland - Martinez ATTN Shelby Lathrop ' Method Volatile Organics Aromatics Batch 6377 Method Code 80208x Analyst evd 1 Surrogate Units 4-Bromofluorobenzene ug/L ' Lab ID Matrix QC Type Dilution Result True Value Percent Recovery Limits Flag Date Time M8 1 45 99 50 0000 92 0 64-147 05/21/1999 1123 LCS 1 45 76 50 0000 91 5 64-147 05/21/1999 1241 990876-8 Solid 1 39 69 50 0000 79 4 64-147 05/21/1999 1514 990876-22 Solid 1 42 18 5D 0000 84 4 64-147 05/21/1999 1540 990876-26 Solid 1 41 41 50 0000 82 8 64-147 05/21/1999 1606 990876-29 Solid 1 43 66 50 0000 87 3 64-147 05/21/1999 1632 990876-30 Solid 1 42 61 50 0000 85 2 64-147 05/21/1999 1658 ' 990876-32 Solid 1 38 58 50 0000 77 2 64-147 05/21/1999 1724 990865 19 Solid 1 37 75 50 0000 75 5 64-147 05/21/1999 1934 LCD 1 49 62 50 0000 99 2 64-147 05/21/1999 2000 990865 22 Solid 1 34 24 50 0000 68 5 64 147 05/21/1999 2210 990877-3 Solid 1 44 75 50 OOOC 89 5 64 147 05/21/1999 2236 0877-4 Solid 1 46 31 50 0000 92 6 64 147 05/21/1999 2302 0877-5 Solid 1 44 83 50 0000 89 7 64-147 05/21/1999 2328 0877-6 solid 9 43 20 50 0000 86 4 64-147 05/21/1999 2354 990877-7 Solid 1 48 26 50 0000 96 5 64-147 05/22/1999 0020 990877-9 Solid 1 49 18 50 0000 98 4 64-147 05/22/1999 0046 990877-11 solid 1 41 94 50 0000 83 9 64-147 05/22/1999 0112 990877-12 Soitd 1 47 14 50 0000 94 3 64-147 05/22/1999 0138 990877 5 Solid MS 1 46 21 50 0000 92 4 64-147 05/22/1999 0321 ' 990877 5 Solid MSO 1 46 09 50 0000 92 2 64-147 05/22/1999 0347 Method — f Volatile Orgam cs Aromatics Batch 6380 Method Code 8020BX Analyst cvd Surrogate Units ' 4 Bromofluorobenzene ug/L Lab ID Matrix CC Type Dilution Result True Value Percent Recovery Limits Flag Date Time M8 1 43 46 50 0000 86 9 64-147 05/22/1999 0505 LCS 1 45 55 50 0000 91 1 64-147 05/22/1999 0623 LCD 1 44 60 50 0000 89 2 64-147 05/22/1999 0649 990877-16 Solid 1 42 88 50 0000 85 8 64-147 05/22/1999 0715 ' 990877 17 Solid 1 44 79 50 0000 89 6 64-147 05/22/1999 0741 990877-22 Solid 1 51 74 50 0000 103 5 64-147 05/22/1999 0859 990890-1 Solid 1 44 62 50 0000 89 2 64-147 05/22/1999 0952 990890-2 Solid 1 44 91 50 0000 89 8 64-147 05/22/1999 1018 ' 990890-3 Solid i 42 43 50 OOOO 84 4 64 147 05/22/1999 1044 990885-1 Solid 1 144 00 50 0000 288 0 64-147 x 05/22/1999 1110 990890-3 Solid MS 1 45 79 50 0000 91 6 64-147 05/22/1999 1227 990890-3 Solid MSD 1 43 43 50 0000 86 9 64-147 05/22/1999 1253 Page 46