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L CORE LABORATORIES Job Number: 981535 Date: 10/30198 ........... .......... tusjowk. f uor. Dante.l STi R..R.O..J..EC�T. .................. . ....Shelby..........Lathrop ............. ............. ATTN ........... :7 is�rs sm ................................................................. QC Type Description Reag- Code Lab ID Dilution Factor Date Time .... .......... . . ............................ ............................... ..................................... .......................... .................... .......... Parameter/Test Description OC Result QC Result True Value Orig. Value Calc. Result Limits nzene 5.156 0.50 Ethytbenzene 0 0.50 methyt-t-Butyl Ether (MTBE) 0 10.00 LOLuene 3.140 0.50 Lenes (total) 0.00 0.50 .................... Lahorat ............. oV.:.:C...o.h..t..f.b..L..Sample ............ . .r. .:1. : ....:.."...............:.......................... ........................................ ..................... ........ ... ............... 10/14/98 D722.; ..... .............. .... ...... L Parameter/Test Description QC Result OC Resu i t True Value 0 rig Value Calc. Result Limits A Cnzene 24.478 20. 122.4 % 39-150 hytbenzene 24.035 20- 120.2 % 32-160 thyL-t-ButyL Ether (MTBE) 59.112 20. 295.6 % 50-150 Toluene 23.790 20. 119.0 % 46-148 -!nes (total) 69.80 60. 116.3 % 75-125 MS Matrix 5/ 98034 0$082701 981535 :21 a 0/1 . :' .0 ' Spike ....................................... .................. . ...... . . . . . Parameter/Test Description QC Result QC Result True Value orig. Value Calc. ResuLt Limits Lenzene 20,336 20. 0 101.7 % 39-150 EthyLbenzene 18.924 20. 0 94.6 % 32-160 Methyl-t-Butyl Ether (MTBE) 68.292 20. 42.515 128.9 % 50-150 Luene 19.813 20. 1.821 90.0 % 46-148 lenes (total) 57.25 60. 4.80 87.4 % 75-125 ........... :7 35- ....... MatrEx Spike 8.:.::..X)1q0 msinsiisi MSD .......... L Parameter/Test Description OC Result QC Result True Value Orig. Value Calc. Result Limits Benzene 20.999 20.336 20. 0- 105.0 % 39-150 3 R 20 L'-hyLbenzene 19.122 18.924 20. 0 95.6 % 32-160 1 R 20 Methyl-t-Butyl Ether (MTBE) 71.153 68.292 20- 42.515 143.2 % 50-150 4 R 25 A luene 20.221 19.813 20. 1.821 92.0 % 46-148 L 2 R 20 Xylenes (total) 57.92 57.25 60. 4.80 88.5 % 75-125 1 R 20 CCV ................ C.6nf nui ng�Cai '6r cati: 10/15/98"""0245 ':: on, '. a Parameter/Test Description QC Result QC Result True Value orig. Value Calc. Result Limits ene 22.479 20. 112 % 85-115 Lbenzene 20.312 20. 102 % 85-115 hyl-t-Butyl Ether (MTBE) 52.551 20. 263 % 85-115 COULA h L luene 21.392 20. 107 % 85-115 Page 36 REC R-RPD A-ABS Diff. 0-7 Diff.