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Report Number 35062 QC Report Matrix Spike! Matrix Spike Duplicate Date 9/29/2003 I Project Name 7-Eleven Store #14117 Project Number 77EL 14117.03 Duplicate Spiked Duplicate Spiked Spiked Sample Relative Spike Spiked Spiked Sample Sample Relative Percent Percent Spiked Sample Spike Dup Sample Sample Analysis Date Percent Percent Percent Recov Diff Parameter Sample Value Level Level Value Value Units Method Analyzed Recov Recov Diff Limit Limit Benzene 34973-09 <0 50 400 400 36 7 354 uglL EPA 8260B 9123103 918 88 4 3 69 70-130 25 Toluene 34973-09 <0 50 400 400 362 353 ug/L EPA 8260B 9123103 90 6 882 260 70-130 25 Tert-Butanol 34973-09 <5 0 200 200 191 191 uglL EPA 82608 9123103 954 954 000 70-130 25 Methyl-t-Butyl Ether 34973-09 065 400 400 396 38 8 ug/L. EPA 8260B 9123103 973 954 197 70-130 25 Benzene 35153-04 <0 50 400 400 41 7 41 7 uglL EPA 8260B 9129103 104 104 0 144 70-130 25 Toluene 35153-04 <0 50 400 400 422 41 7 uglL EPA 8260B 9129103 105 104 1 02 70-130 25 Tert-Butanol 35153-04 <5 0 200 200 206 204 ug1L EPA 82606 9129103 103 102 0 982 70-130 25 Methyl-t-Butyl Ether 35153-04 <0 50 400 400 41 7 406 ug/L EPA 82608 9129103 104 102 265 70-130 25 Benzene 35144-02 4 1 400 400 434 41 6 uglL EPA 82606 9126103 98 3 938 468 70-130 25 Toluene 35144-02 <0 50 400 400 440 427 uglL EPA 8260B 9126103 110 107 295 70-130 25 Tert-Butanol 35144-02 <5 0 200 200 207 207 ug1L EPA 82606 9126103 104 103 0 222 70-130 25 Methyl-t-Butyl Ether 35144-02 82 400 400 120 119 ug1L EPA 82606 9126103 94 2 91 3 310 70-130 25 Benzene 35144-05 <0 50 400 400 41 5 39 3 uglL EPA 8260B 9126103 104 98 3 539 70-130 25 Toluene 35144-05 <0 50 400 400 370 378 uglL EPA 8260B 9126103 924 94 6 238 70-130 25 Tert-Butanol 35144-05 <5 0 200 200 212 211 uglL EPA 8260E 9126103 106 105 0 525 70-130 25 Methyl-t-Butyl Ether 35144-05 <0 50 400 400 41 3 42 9 uglL EPA 82606 9126103 103 107 3 82 70-130 25 Benzene 35028-02 7 2 400 400 480 473 uglL EPA 82606 9123103 102 100 168 70-130 25 Toluene 35028-02 <0 50 400 400 41 2 404 ug/L EPA 8260B 9123103 103 101 2 08 70-130 25 1,,kk, Approved By 1J I � KIFF ANALYTICAL, LLC j 2795 2nd St, Suite 300 Davis, CA 96616 530-297-4800 �,