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OULAB CORE LABORATORIES <br /> 16 <br /> QUAL I T Y C O N T R O L R ESU L T S <br /> Job Number 981689 Date 11/11/98 <br /> CUSTOMER. fluor Daniel GTI PROJECT SL/STOCKTON 420632 ATTN. Shelby Lathrop <br /> QC Type Description Reag Code Lab ID Dilution Factor Date Time <br /> 1NSD Matrix Spike Duplicate M7022223 981692-9 11/04/98 2016 <br /> Parameter/Test Description QC Result QC Result True Value Orig Value Calc Result * Limits <br /> ad 2 84124 3 84689 5 0 0 08844 55 % 75-125 <br /> 30 1 R 20 <br /> Magnesium (Mg) 123 13390 124 20274 5 0 116 09254 141 % 75-125 <br /> 0 9 R 20 <br /> tybdenum <br /> ganese (Mn) 6 35873 7 37899 5 0 3 33970 60 % 75-125 <br /> 14 9 R 20 <br /> 3 66134 3 38133 5 0 0 03010 73 % 75-125 <br /> 80 R20 <br /> ickel 2 95018 3 91639 5 0 0 14721 56 % 75-125 <br /> 28 1 R 20 <br /> [icon (Si) 2605 92382 2728 05859 5 0 3137 22314 10626 % 75-125 <br /> 4 6 R 20 <br /> etenium 4 13861 5 18170 5 0 1 25792 58 % 75-125 <br /> 22 4 R 20 <br /> )dium (Na) 9 20900 9 71985 5 0 4 77478 89 % 75-125 <br /> 54 R20 <br /> Si ver 1 90208 2 03450 5 0 -0 00251 38 % 75-125 <br /> 6 7 R 20 <br /> tium (Sr) 3 56455 4 53901 5 0 0 65005 58 % 75-125 <br /> io <br /> 24 1 R 20 <br /> Thatlium 2 71354 3 74178 5 0 -0 03450 55 % 75-125 <br /> 31 9 R 20 <br /> n (Sn) 3 68763 3 40118 5 0 0 09012 72 % 75-125 <br /> 8 1 R 20 <br /> lanad i ur 3 43269 4 43405 5 0 0 61432 56 % 75-125 <br /> 25 5 R 20 <br /> nc 3 43629 4 40134 5 0 0 68320 55 % 75-125 <br /> 24 6 R 20 <br /> CCV Continuing Calibration verification M7022223 17/04/98 2112 <br /> Parameter/Test Description QC Result QC Result True Value Orig Value Calc Result * Limits <br /> Aluminum (AL) 5 18740 5 0 104 % 90-110 <br /> timony 4 93139 5 0 99 % 90-110 <br /> senic 5 02326 5.0 100 % 90-110 <br /> ryttium 4 99736 5 0 100 % 90-110 <br /> Boron (B) 4 98361 5 0 100 % 90-110 <br /> Odmium 5 06329 5 0 101 % 90-110 <br /> lctum (Ca) 5 22596 5 0 105 % 90-110 <br /> romium 5 02058 5 0 100 % 90-110 <br /> 'baLt 5 03699 5 0 101 % 90-110 <br /> Copper 4 89541 5 0 98 % 90-110 <br /> Ion (Fe) 5 30190 5 0 106 % 90-110 <br /> ad 5 01739 5 0 100 % 90-110 <br /> gnesium (Mg) 5 09850 5 0 102 % 90-110 <br /> Manganese (Mn) 5 00305 5 0 100 % 90-110 <br /> tybdenum 4 96914 5 0 99 % 90-110 <br /> ickel 5 OZ175 5 0 100 % 90-110 <br /> ilicon (Si) 59 78240 5 0 1196 % 90-110 <br /> �in 4 98617 5 0 100 % 90-110 <br /> (Na) 4 93339 5 0 99 % 90-110 <br /> ' Page 25 <br /> * %-% REC R-RPD A-ABS Diff D-% Diff <br /> Tme—0F 1­1 M­ a Mr p stet ma cont n�n ins nppn p W ed upo W mal n a-d—11 n epp eo by rn._c en fhk wr .no-vu end u t]car 1,v n r m tle rl. y u I rp.n.N. i warj I Y <br /> was so epe r the pe r <br /> '9—of Cwe wlw'e—,�Gae ww;e e noewce r mnkn o wa afry a ewe--w w,.p e:. o mp ra ntr�y Iw ra e o® 7 o s.,m .mme a ro r^`Wpnn.n InY woo nR rl o a wog r cmo eor <br /> 6 }1 p Cines mne t�0 ppe 1Y�e o �M neCl O w M n CpeYt u.nt)W rc ed"PC"to a y e wnat pp port s a �r Oe epW�crd wre e p * er ipp w.,i or Co a �b <br />