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1 <br /> 10 LAB CORE LABORATORIES <br /> 0 U A L I T Y C 0 M T R 0 L R E S U L T S <br /> Job Number 981689 Date 11/11/98 <br /> CUSTOMER Fluor Daniel GTI PROJECT. SL/STOCKTON #20632 ATTN. Shelby Lathrop <br /> QC Type Description Reag Code Lab ID Dilution Factor Date Time <br /> Test Method EPA 8260B Batch 3588 Analyst vz <br /> Method Description Volatile Organics by GC/MS Units ug/L <br /> Ma Method Blank 11/04/98 1711 <br /> Parameter/Test Description QC Result QC Result True Value Orig Value Calc Result * Limits <br /> rt-Butyl Alcohol (TBA) 0 100 <br /> i-Isopropyl Ether 0 5 00 <br /> Ethyl tent-Butyl Ether (ETBE) 0 5 00 <br /> rt-Amyl Methyl Ether 0 5 00 <br /> thyl-t-Butyl Ether (MTBE) 0 10 00 <br /> SB Spiked Blank 08092101 1090 11/04/98 2144 <br /> Parameter/Test Description QC Result QC Result True Value Orig Value Calc Result * Limits <br /> tert-Butyl Alcohol (TBA) 308 20 500 000000 61 6 % 75-125 <br /> propyl Ether 21 37 25 000000 85 5 % 75-125 <br /> tert-Butyl Ether (ETBE) 13 05 25 000000 52 2 % 75-125 <br /> rt-Amyl Methyl Ether 9 54 25 000000 38 2 % 75-125 <br /> Methyl-t-Butyl Ether (MTBE) 34 80 50 000000 69 6 % 75-125 <br /> SBD Spiked Blank Duplicate 08092101 1000 11/04/98 2214 <br /> Parameter/Test Description QC Result QC Result True Value Orig Value Calc Result * Limits <br /> rt-Butyl Alcohol (TBA) 319 59 308 20 500 000000 63 9 % 75-125 <br /> 3 6 R 20 <br /> Di-Isopropyl Ether 20 67 21 37 25 000000 82 7 % 75-125 <br /> 3 3 R 20 <br /> hyl tert-Butyl Ether (ETBE) 13 31 13 05 25 000000 53 2 % 75-125 <br /> 20 R20 <br /> lert-Amyt Methyl Ether 9 21 9 54 25 000000 36 8 % 75-125 <br /> 35 R20 <br /> thy[-t-Butyl Ether (MTBE) 32 75 34 80 50 000000 65 5 % 75-125 <br /> 6 1 R 20 <br /> CV Continuing Calibration Verification 08092101 1000 11/04/98 1635 <br /> Parameter/Test Description QC Result QC Result True Value Orig Value Calc Result * Limits <br /> tert-Butyl Alcohol (TBA) 413 77 500 000000 83 D 75-125 <br /> isopropyl Ether 23 87 25 000000 95 D 75-125 <br /> hyl tert-Butyl Ether (ETBE) 25 21 25 000000 101 D 75-125 <br /> rt-Amyl Methyl Ether 23 91 25 000000 96 D 75-125 <br /> Methyl-t-Butyl Ether (MTBE) 44 89 50 000000 90 D 75-125 <br />' Page 30 <br /> * %-% REG R-RPO A-ABS Diff D-% Diff <br /> Tne a aiytrCl a.0 Is ov ane a nl p etas MS ja w n to s 4iwn—b-1—nt �p e by the c MI I«who c u d a a t,onldnnl r to owl U xr h c ni yt oP c+ «nlmc ula itl� <br />' a.Al¢'vea ep v,Bn11n0 Oe5liggmMl Of C«c 1.atl«JIon0. W0 tib«oto u Wwwc m.lhl�np wa untY n [�C-.Bnt�lan p'B' «�mP W of nv IYnk aM asA e I 0 I-rl n w �e a In ne p ct a raYOG ope I anti p p pf I..b at <br /> uny p Wa 4o�i«pin0 rc ..I WoWy w —n t wn CN s h q t 5 uxM W t etl p «u�ry ma whit p Yn egdt „ nl bn YP'W c P t rap. Pf Ctr0 LWn oto e <br />