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L�4B CORE LABORATORIES to M -- Q U A L I T Y C 0 N T R 0 L R E S U L T S Job Number 981801 Date 11/20/98 USTOMER. Fluor Daniel GTi PROJECT. 5l./STOCKTON/20632 ATTN. Shelby Lathrop QC Type Description Reag Code Lab ID Dilution Factor Date Time Test Method EPA 8015Mod Batch 3697 Analyst .. evd Method Description Total Volatile Petroleum Hydrocarbons Units ug/L 5 Matrix Spike 08110203 981801-1 11/18/98 0033 Parameter/Test Description QC Result QC Result True Value Orig Value Calc Result * Limits saline Range Petroleum Hydrocarbons 946 57 1000 0 103 52 84 % 50-150 SD Matrix Spike Duplicate 08110203 981801-1 11/1$/98 0100 Parameter/Test Description QC Result QC Result True Value Orig Value Calc Result * Limits saline Range Petroleum Hydrocarbons 1012 73 946 57 1000 0 103 52 91 % 50-150 1 6 8 R 20 Test Method EPA 8015 Mod Batch 3716 Analyst evd Method Description Total Extractable Petroleum Hydrocarbons Units mg/L 14S Matrix Spike 08090801 981792-12 11118198 1631 Parameter/Test Description QC Result QC Result True Value Orig Value Calc Result * Limits TEPH - as Diesel 1079 59 1000 0 108 % 50-150 MSD Matrix Spike Duplicate 08090801 981792-12 11/78/98 1713 Parameter/Test Description QC Result QC Result True Value Orig Value Calc Result * Limits PH as Diesel 1082 54 1079 59 1000 0 108 % 50-150 0 3 R 20 Test Method EPA 8260B Batch 3718 Analyst vz Method Description Volatile Organics by GC/MS Units ug/L SIS Matrix Spike 08092101 981801-2 1000 1117/98 1729 Parameter/Test Description QC Result QC Result True Value Orig Value Calc Result * Limits rt-Butyl Alcohol (TBA) 422 55 500 000000 0 84 5 % 75-125 Isopropyl Ether 21 34 25 000000 0 85 4 % 75-125 Ethyl tert-Butyl Ether (ETBE) 21 78 25 000000 0 87 1 % 75-125 tert-Amyl Methyl Ether 23 03 25 000000 0 92 1 % 75-125 thy!-t-Butyl Ether (MTBE) 40 14 50 000000 0 80 3 % 75-125 I Page 9 * %-% REC R-RPD A-ABS Diff D-% Diff ine s nIN cal {s o0 em b nl eyp Blal ons can!-n6a Int eapl a a if ea ppn nfwm t`n d meter I t pP op ny the c a t to who{e exeu e a tl cool tlan1J u e II, epo 1 ny pgan-d,The an elyl C0110 111 aP-a a n•p v[a t•m exp N"pd Iq ePenl ine tM I.u0mpll o}Cpe LaWratP ies Cpe Lahti x{p es Iwwmn m k wa �n1y p r{e r 1_{ pro n mp o0 OI any IYpll and®p e ly d.cLc mg game as 101 0 o0oct rf1V pope op[allp a pot t_CY+re 4 0l ' any o 9t cP r w Otnel m�rJ pppedy we d SSntl COnnOcl M wt1M1 rvM1 Ch SocM1 Cpo 5 u ed w e ed apo +w ny a 5Pn wnllyoaver Thy epo 1 sou w+be ePOOtrcep n wlpla d n port wlindA Ine wt Ileo app•aysl o!�e Lobo a1a1w+