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WEST COAST ANALYTICAL SERVICE, INC. <br /> 16 NET PACIFIC Job # 17711 <br /> Ms. Kelly Temple February 11, 1991 <br /> LABORATORY REPORT <br /> TABLE 2 <br /> Parts Per-Million <br /> OC Summary <br /> Sample 5829-73480 <br /> MS <br /> Ethylene Propylene <br /> Glycol Glycol <br /> Amount in Sample ND ND <br /> Amount Found 9. 0 10.5 <br /> Amount Spiked 11.06 10.76 <br /> Percent Recovered 81t 97.5% <br /> ND-Not Detected <br /> TEXT <br /> The samples were analyzed on a Varian 6000 gas chromatograph <br /> equipped with a flame ionization detector (FID) . A 30m x 0. 53r-m <br /> DB wax megabore column was used with temperature programming from <br /> 500C to 1500C at 10°C/min. <br /> Five (5) grams of soil sample was weighed out and extracted with <br /> five (5) ml of water. <br /> Direct aqueous injection was used with a five (5) point <br /> 1 calibration curve to standardize the instrument. A water blank <br /> was used as the method blank. <br /> Page 3 of 3 <br />