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1 M • <br /> Entech Analytical Labs, Inc. <br /> 1 3334 Victor Court , Santa Clara, CA 95054 Phone: (408) 588-0200 Fax: (408) 588-0201 <br /> 1 Frey Environmental Date: 11/18/2003 <br /> 2817 ALaFayette Avenue Date Received: 11/14/2003 <br /> Project Name: Ryder <br /> Newport Beach,CA 92663 <br /> ProjectNumber: 053-06 <br /> Attn: Evan Privett P.O.Number: <br /> Certified Analytical Report Sampled By: <br /> 1 Order ID: 36587 Lab Sample ED: 36587-003 Client Sample ID: D8-2 <br /> Sample Time: 12:00 PM Sample Date: 11/14/2003 Matrix: Solid <br /> Extraction Analysis <br /> 1 Parameter Result Flag DF PQL DLR Units Date Date QC Batch ID Method <br /> Benzene ND 1 5 5 µg/Kg N/A 11/17/2003 SMS310356C EPA 8260B <br /> Ethyl Benzene ND 1 5 5 pg/Kg N/A 11/17/2003 SMS310356C EPA 8260B <br /> ' Toluene ND 1 5 5 gg/Kg N/A 11/17/2003 SMS310356C EPA 8260B <br /> Xylenes,Total ND 1 5 5 pg/Kg N/A 11/17/2003 SMS310356C EPA 8260B <br /> Surrogate Surrogate Recovery Control Limits(%) <br /> 4-Bromofluorobenzene 77.2 70 - 130 <br /> 1 Dibromofluoromethane 92.8 59 - 134 <br /> Toluene-d8 86.8 60 - 112 <br /> ' Extraction Analysis <br /> Parameter Result Flag DF PQL DLR Units Date Date QC Batch ID Method <br /> tert-Butanol(IBA) ND 1 20 20 pg/Kg N/A 11/17/2003 SMS310356C EPA 8260E <br /> 1 Methyl-t-butyl Ether ND 1 5 5 µg/Kg N/A 11/17/2003 SMS310356C EPA 8260B <br /> Diisopropyl Ether ND 1 5 5 µg/Kg N/A 11/17/2003 SMS310356C EPA 8260B <br /> Ethyl-t-butyl Ether ND 1 5 5 pg/Kg N/A 11/17/2003 SMS310356C EPA 8260B <br /> ' tert-Amyl Methyl Ether ND 1 5 5 µg/Kg N/A 11/17/2003 SMS310356C EPA 8260B <br /> Surrogate Surrogate Recovery Control Limits(%) <br /> 4-Bromofluorobenzene 77.2 70 - 130 <br /> 1 Dibromoflumomethane 92.8 59 - 134 <br /> Toluene-d8 86.8 60 - 112 <br /> 1 . <br /> 1 <br /> 1 <br /> 1 DF=Dilution Factor ND=Not Detected DLR=Detection Limit Reported PQL=Practical Quantitation Limit <br /> / I�/ 03 u.,.-f I I / I s/ 03 <br /> Analyst Date Supervisor Date <br />