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` CASTLE ANALYTICAL LABORATORY - PORTERVILLE <br /> Environmental Testing Services 2780 Yowlumne Ave.,Suite C phone: (559)781-6099 <br /> Porterville,CA 93258 Fax: (559)781-6091 <br /> Sherwood Labs Corporation Client Project ID: Georges Service Sample Prep Method: SW3050 <br /> P.O. Box 937 Reference Number: P1701 6162 Analysis Method: SW6010C <br /> Hilmar,CA 95324 Sample Description;SOIL Prepared: 10-03-03 <br /> Attn:Vicki Hubis Instrument ID:TJA 61E Analyzed: 10-06-03 <br /> Repotted: 10-07-03 <br /> QUALITY CONTROL DATA REPORT <br /> SPIKE ID: ICP 0033-1 <br /> Reporting BLANK Spiking Control %R <br /> { Limit Result Level Spike Limits <br /> m Ik mg/kg rn Ik %R <br /> COMPOUNDS <br /> .. I Lead 5.0 ND 62.5 8b.5% 80-120 <br /> Spiking MATRIX MATRIX %R %RPD <br /> Level SPIKE SPIKE DUP Limits <br /> m /k %R %R <br /> COMPOUNDS <br /> Lead 62.5 65.6% 68.0% 70-130 1.80% <br /> I <br /> i <br /> I <br /> L i <br /> r <br /> lF' <br /> The LCS(Laboratory Control Spike)is a control sample of known,interferent free matrix that is fortified with representative analytes and <br /> analyzed using the same reagents,preparation and analytical methods employed for the samples. The LCS%recovery is used for validation <br /> of sample batch results. Due to matrix effects,the QC limits and recoveries for MSIMSD's are advisory only and are not used to accept or <br /> reject batch results. <br /> APPROVED B ; <br /> J mei C.Phillips I <br /> aboratory Director <br /> t <br />