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' Air,Water&hazardous Waste Samphn&Analysis&Consultation <br /> COAST TO - Certzfted Hazardous Waste,Chemistry,Bacteriology&Bioassay Laboratories <br /> COAST <br /> San Luis Olnspo,CA -Goleta,CA -Becuaa,CA-Camarillo,CA-Newport Beach,CA-Valparaiso,114 <br /> Benicia Division (707) 747--2757 <br /> 6006 Egret court, Benicia, California 94510 FAX (707)747-2765 <br /> QC Batch ID: BDD14I1 <br /> CLIENT: coast-oto-coast Analytical Services, Inc. <br /> Analyzed : 04/14/92 <br />' Analyzed by: AZ <br /> Method As Listed <br /> QC SPIKE <br /> REPOW OF ANALYTICAL RESULTS Page 1 of 1 <br /> SAMPLE DESCRIPTION MATRIX SAMPLED BY SAMPLED DATE RECEIVED <br /> ' QC SPIV DUP'LICA'TE Aqueous <br /> *PCZ. SPII{E RESULT �rREC $DIFF NOTE <br /> CONSTITUENT <br /> FUEL FINGERPRINS ANALYSIS 1,2 <br /> Benzene 0.5 180. 200. 111. 0. <br /> ' Toluene 0.5 710. 730. 103. 0. <br /> Ethylbenzene 0.5 170. 160. 94. 6.1 <br /> Xylenes 0.5 810. 810. 100. 3.6 <br /> 1,2-Dichlaroethane (EDC) 0.5 NS <br /> Ethylene Dibrcmide (IDB) 0.5 NS <br /> Total Petroleum Hydrocarbono (Gasolin2; 50. 7100. G000. 85. 4.9 <br /> Total Petroleum Hydrocarbons (Diesel 2) 50. NS <br /> ' BTX as a percent of fuel 24. 29. <br /> Peru Surrogate Recovery 100. 102. <br /> 1,2-Dichlomethane-d4 (Su=;Ogate) 100. 115. 115. 1.7 <br /> Toluene-d8 (Surrogate) 100. 98. 98. 0. <br /> p^Bromofluorobenzem (Surmgats) 100. 92. 92. 3.2 <br /> ' Benicia Division Lab Certifications: CM2M #1719; L.A.Co.CSD#10185 <br /> * RESULTS listed, as 'NS' were not spiked. PQi. = Practical Quantitation Limit <br /> (1) ANALYZED by CAL DOLS DRAFT TPH (modified) and EPA 8260 (GC/MS) <br /> ' (2) EXTRACIED by EPA 5030 (purge-and-trap) <br /> ' <br /> 04/23/92 Respectfully submitted, <br /> INOOS 50-387 C04ST-TO-CMSST�YIANALYTICAL SERVICES, M. ' <br /> MH/txk/htc G' ' <br /> ED0187-3 <br /> Mary Ha icek, Ph.D. <br /> President <br />