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Alpha Analytical, Inc. <br /> 255 Glendale Ave. •Suite 21 • Sparks,Nevada 89431-5778 <br /> (775) 355-1044 •(775)355-0406 FAX• 1-800-283-1183 <br /> Work Order: <br /> OC Surmnary Report 03061929 <br /> 3 a-Jun-0.3 <br /> Method Blank Type MBLK Test Code: EPA Method SW8260B <br /> File ID: D:IHPCHEM1MS091DATA1030620103062006.0 Batch ID:MS9W0620A Analysis Date: 06120!2003 11:32 <br /> Sample ID: MBLK MS9W0620A Units : µglL Run ID:GCIMSD_9_030620A Prep Date: 0612012003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPD Ref Val %RPD Qual <br /> Tertiary Butyl Alcohol(TBA) ND 5 <br /> Methyl tent-butyl ether(MTBE) ND 0.5 <br /> Di-isopropyl Ether(DIPE) ND 1 <br /> Ethyl Tertiary Butyl Ether(ETRE) ND 1 <br /> 1,2-Dichloroethane ND 1 <br /> Benzene ND 0.5 <br /> Tertiary Amyl Methyl Ether(TAME) ND 1 <br /> Toluene NO 0.5 <br /> 1,2-Dibromoethane(EDB) ND 2 <br /> Ethylbenzene ND 0.5 <br /> m,p-Xylene ND 0.5 <br /> o-Xylene ND 0.5 <br /> Surr: 1,2-Dichloroethane-d4 9.26 1D 93 72 126 <br /> Surr.Toluene-d8 9.79 10 98 71 128 <br /> Surr:4-Brom ofluoro benzene 8.81 10 88 76 121 <br /> Laboratory Control Spike Type LCS Test Code'. EPA Method SWB260B <br /> File ID: D:XHPCHEMIMS091DATA1030620103062004.D Batch ID:MS9W0620A Analysis Date: 0612012003 10:45 <br /> Sample ID: LCS MS9W0620A Units:NglL Run ID:GCIMSD_9_030620A Prep Date: 0612012003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPD Ref Val %RPD Qual <br /> Benzene 11 0.5 10 110 83 119 <br /> Toluene 10.1 0.5 10 101 80 120 <br /> Oylbenzene 9.9 0.5 10 99 80 120 <br /> Xylene 17.6 0.5 20 88 77 124 <br /> ylene 9.36 0.5 10 94 77 125 <br /> Surr:1,2-Dichloroethane-d4 9.07 10 91 72 126 <br /> Surr.Toluene-d8 9.97 10 9 71 128 <br /> Surr.4-Bromofluorobenzene 9.55 10 966 76 121 <br /> Sample Matrix Spike Type MS Test Code: EPA Method SW8260B <br /> File ID: D:IHPCHEMIMS091DATA1030620103062007.D Batch ID: MS9W0620A Analysis Date: 06/20/2003 11:56 <br /> Sample ID: 03061920-01AMS Units: pgIL Run ID:GCIMSD_9_030620A Prep Date: 06120/2003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPD Ref Val %RPD Qual <br /> Benzene 55.2 1.3 50 0 110 83 119 <br /> Toluene 48 1.3 50 0 96 80 120 <br /> Ethylbenzene 48 1.3 50 0 96 80 120 <br /> 85.3 1.3 100 0 85 77 124 <br /> m,p-Xylene <br /> rnp-X le 44.6 1.3 50 0 89 77 125 <br /> o-XyleSurr:1,2-Dichloroethane-d4 46 50 92 72 126 <br /> S49.2 50 98 71 128 <br /> urr:Toluene-dB <br /> 47.2 50 94 76 121 <br /> Surr:4-Bromofluorobenzene <br /> Sample Matrix Spike Duplicate Type MSD Test Code: EPA Method SW8260B <br /> File ID: D:IHPCHEMIMS091DATAI030620103062008.D Batch ID:MS9W0620A Analysis Date: 06/20/2003 12:20 <br /> Sample ID: 03061920-01AMSD Units : pg1L Run ID:GCIMSD_9_030620A Prep Date: 0612012003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPD Ref Val %RPD Qual <br /> Benzene 57.9 1.3 50 0 116 83 119 55.16 4.81 <br /> Toluene 50.3 1.3 50 0 101 80 120 47.95 4.68 <br /> Tne <br /> olue50.1 1.3 50 0 100 60 120 47.97 4.38 <br /> Ethylbenzene enzene 87.9 1.3 100 0 88 77 124 85.29 2.96 <br /> m,P-X le 46.5 1.3 50 0 93 77 125 44.56 4.26 <br /> o-XyleSurr:1,2-Dichloroethane-d4 44 50 88 72 126 <br /> rr:Toluene-dB 49.6 50 99 71 12B <br /> r:4-Bromofluorobenzene 46.5 50 93 76 121 <br />