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Alpha Analytical, Inc. 255 Glendale Ave. • Suite 21 • Sparks, Nevada 89431-5778 (775) 355-1044 • (775) 355-0406 FAX • 1-800-283-1183 • ,la QC Summar Report Work Ordcr: �<< W y p 01100400 N'lethod Blank Type MBLK Test Code: SW8015 Batch ID:MS8W1005B Fiie ID D:(HPCHEM1MS081DATAl0i1005101100506.D Analysis Date: 10105/2001 11:46 Sample ID MBLK MS8W1005A Units : mglL Run ID:GCIMSD_8_011005A Prep Date: 1010512001 Analyte Result PQL SpkVal SpkRefVal %REC LoWLimit HighLimit RPD Ref Val %RPD Qual TPri Purgeabie ND 0.05 Surr 1.2-Dichloroethane-04 0.0104 0.01 104 71 130 Surr Toluene-d8 0.00961 0.01 98 69 127 Surr 4-Brornofluorobenzene 0.0115 0.01 115 80 123 Laboratory Control Spike Type LCS Test Code: SW8015 Batch ID:MS8W1005B Fne ID D:IHPCHEMIMS08\DATA1011005101100505.D Analysis Date: 10/05/2001 11:22 Sample ID' GLCS MS81005A Units:mg1L Run ID:GCIMSD_8_011005A Prep Date: 10/0512001 Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPD Ref Val %RPD Qual TPH Purgeable 0.43 0.05 0.4 107 58 136 Surr 1,2-Dichloroethane-d4 0.01 0.01 100 71 130 Surr:Toluene-d8 0.00892 0.01 89 69 127 Surr 4-Bromofluorobenzene 0.011 0.01 110 80 123 Sample Matrix Spike Type MS Test Code: SW8015 Batch 0:MSBW1005B File ID: D:IHPCHEM%MS081DATA1011005\01100509.13 Analysis Date- 10/05/2001 12:59 Sample ID: 01100466-02AGS Units: mg/L Run ID:GC/MSD_8_011005A Prep Date: 1010512001 Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPD Ref Val %RPD Qua[ TPH Purgeable 2.26 0.25 2 0.1891 104 58 136 Surr 1,2-Dichloroethane-d4 0.0514 0.05 103 71 130 Surr Toluene-d8 0.0427 0.05 85 69 127 ,gMkSurr 4-Bromoftuorobenzene 0.054 0.05 108 80 123 Sample Viatrix Spike Duplicate Type MSD Test Code: SW8015 Batch ID:MS8W1005B Foe ID D 1HPCHEM\MS081DATA101100510i100510.D Analysis Date 10/05/2001 13:24 Sample ID 01100466-02AGSO Units . mg/L Run ID.GCIMSD_8_011005A Prep Date. 1010512001 Anayte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPD Ref Val %RPD Qual TPH Purgeable 2.38 0.25 2 0.1891 109 58 136 2.261 5.45 Surr 1,2-Dichloroethane-d4 0.0509 0.05 102 71 130 Surr Toluene-d8 0.0438 0.05 88 69 127 Surr 4-Bromoftuorobenzene 0.0543 0.05 109 80 123 ( oinmcnts: IND- Not Detected at the Reporting Limit. D-Ifthe spiked value is X25%of the reference value,recovery should not be calculated. S-Spike Recovery outside accepted recovery limits. M-Spike Recovery outside accepted recovery limits due to matrix. B -Analyte detected in the associated Method Blank.