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Well Purging <br /> 9 J <br /> Before sampling occurred, a polyvinyl chloride (PVC) bailer, centrifugal pump, low-flow <br /> submersible pump, or Teflon bailer was used to purge standing water in the casing and <br /> gravel pack from the monitoring well. Monitoring wells were purged according to the <br /> protocol presented in Figure A-1. In most monitoring wells, the amount of water purged <br /> before sampling was greater than or equal to three casing volumes. Some monitoring <br /> wells were expected to be evacuated to dryness after removing fewer than three casing <br /> volumes. These low-yield monitoring wells were allowed to recharge for up to 24 hours. <br /> Samples were obtained as soon as the monitoring wells recharged to a level sufficient for <br /> sample collection. If insufficient water recharged after 24 hours, the monitoring weII was <br /> recorded as dry for the sampling event. <br /> Groundwater purged from the monitoring wells was transported in a 500-gallon water <br /> trailer, 55-gallon drum, or a 325-gallon truck-mounted tank, to EMCON's San Jose or <br /> Sacramento office location for temporary storage. Pinnacle arranged for transport and <br /> disposal of the purged groundwater through Integrated Waste Stream Management, Inc. <br /> Field measurements of pH, specific conductance and temperature were recorded in a <br /> waterproof field logbook. Figure A-2 shows an example of the water sample field data <br /> . sheet on which field data are recorded. Field data sheets were reviewed for completeness <br /> by the sampling coordinator after the sampling event was completed. <br /> The pH, specific conductance, and temperature meter were calibrated each day before <br /> field activities were begun. The calibration was checked once each day to verify meter <br /> performance. Field meter calibrations were recorded on the water sample field data sheet. <br /> Well Sampling <br /> A Teflon bailer was the only equipment acceptable for well sampling. When samples for <br /> volatile organic analysis were being collected, the flow of groundwater from the bailer <br /> was regulated to minimize turbulence and aeration. Glass bottles of at least 40-milliliters <br /> volume and fitted with Teflon-lined septa were used in sampling for volatile organics. <br /> These bottles were filled completely to prevent air from remaining in the bottle. A <br /> positive meniscus formed when the bottle was completely full. A convex Teflon septum <br /> was placed over the positive meniscus to eliminate air. After the bottle was capped, it was <br /> inverted and tapped to verify that it contained no air bubbles. The sample containers for <br /> other parameters were filled, filtered as required, and capped. <br /> When required, dissolved concentrations of metals were determined using appropriate <br /> field filtration techniques. The sample was filtered by emptying the contents of the Teflon <br /> bailer into a pressure transfer vessel. A disposable 0.45-micron acrylic copolymer filter <br /> was threaded onto the transfer vessel at the discharge point, and the vessel was sealed. <br /> CplE:\TEtCHERT\STOCKTON\QTRLY1sTKNQ199.DOC-9511sg:t A-3 �iKst4 8 <br />