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Environmental Laboratories_ <br /> Working To Restore Nature <br /> ANALYSIS REPORT <br /> Attention John Lane Date Sampled 03-04-93 <br /> RESNA Date Received 03-09-93 <br /> 1710 Main Street BTEX Analyzed 03-16-93 <br /> Escalon, California 95320 TPI-Ig Analyzed 03-16-93 <br /> Project 110200L, Project W036700 TPI-Id Analyzed 03-13-93 <br /> King Island Resort, Stockton Matrix Water <br /> Ethyl Total <br /> Benzene Toluene Benzene Xylenes TPHg TPHd <br /> ppb ppb ppb ppb ppb ppb <br /> Detection Limit 05 05 05 0 5 50 50 <br /> SAMPLE <br /> Laboratory Identification <br /> KIR MW1 ND ND ND ND ND ND <br /> W1303108 <br /> KIR MW2 ND ND ND ND ND ND <br /> W1303109 <br /> KIR MW3 ND ND ND ND ND ND <br /> W1303110 <br /> KIR MW4 150 1 7 21 10 650 390* <br /> W1303111 <br /> KIR MW5 37 ND ND 22 240 ND <br /> W1303112 <br /> `Chromatogram does not match diesel standard <br /> ppb=parts per billion=ug/L=micrograms per Mer <br /> ND=Not detected. Compound(s)may be present at concentrations below the detection limit. <br /> NR=Analysts not requested <br /> ANALYTICAL PROCEDURES <br /> BTEX Benzene,toluene ethylbenzene and total xylene isomers(BTEX)are measured by extractton using EPA Method 5030 <br /> followed by analysis using EPA Method 8020/602,which utilizes a gas chromatograph(GC)equipped with a phototonization detector <br /> (PED)and a flame-ionization detector(FED)in series <br /> TPHg Total petroleum hydrocarbons as gasoline(low to medium boiling points)are measured by extraction using EPA Method 5030, <br /> followed by analysts using modified EPA Method 8015,which utilizes a GC equipped with an FID <br /> TPHd Total petroleum hydrocarbons as diesel(high boiling points)are measured by extraction using EPA Method 3550 for soils and <br /> EPA Method 3510 for water,followed by modified EPA Method 8015 with direct sample injection into a GC equipped with an FID <br /> March 23,1943 <br /> Laboratory Repr6entative Date Reported <br /> RESNA ENVIRONMENTAL LA130RATORY IS CERTIFIED BY THE STATE OF CALIFORNIA <br /> DEPARTMENT OF HEALTH SERVICES AS A HAZARDOUS WASTE TESTING LA30RATORY <br /> (Certification No 1211) <br /> 42501 Albrae Street• Fremont, CA 94538 9 Phone (510) 623-0775 • (800) 247-5223 • FAX (510) 651-8754 <br />