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GeoAnalytical Laboratories, Inc. <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone (209) 572-0900 Fax (209) 572-0916 <br /> CERTIFICATE OF ANALYSIS <br /> Report#1 K267-02 Oxygenates Date 10/04/99 <br /> Date Rec'd 9/24/99 <br />' Candor Earth Technologies Project 1432 Herman & Helens Manna Date Started 9/30/99 <br /> 188 Frank West Circle Date Completed 10/01/99 <br /> Stockton CA 95206 Pp# <br />' Date Sampled 9/23/99 <br /> Sampler Bill A Cook M <br /> Sample ID Lab ID MDL Method Analyte Results Units <br /> 1432-MW4-9/23/99 K35710 1 0 8260 Methyl tertiary-Butyl Ether (MTBE) ND pg/L <br /> 1 0 Ethanol ND <br /> 10 tertiary-Butanol ND <br />' 1 0 Di-isopropyl ether(DIPE) ND <br /> 1 0 Ethyl tertiary-Butyl Ether (ETBE) ND <br /> 1 0 tertiary-Amyl Methyl Ether (TAME) ND <br />' 1432-MW3-9/23/99 K35711 100 8260 Methyl tertiary-Butyl Ether (MTBE) 9400 pg/L <br /> 5 0 Ethanol ND <br />' 50 tertiary-Butanol 290 <br /> 5 0 Di-isopropyl ether (DIPE) ND <br /> 5 0 Ethyl tertiary-Butyl Ether (ETRE) ND <br /> 5 0 tertiary-Amyl Methyl Ether (TAME) 33 <br /> 1432-MW2-9/23/99 K35712 1000 8260 Methyl ternary-Butyl Ether (MTBE) 92000 Pg/L <br />' 5 0 Ethanol ND <br /> 50 tertiary-Butanol ND <br /> 5 0 Di-isopropyl ether(DIPE) ND <br /> 5 0 Ethyl tertiary-Butyl Ether (ETRE) ND <br />' 5 0 tertiary-Amyl Methyl Ether(TAME) 520 <br /> I <br /> Cr <br /> I <br /> 1 Sylvia Krenn Donna Keller <br /> Chemist Certification # 1157 Laboratory Director <br />