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r 110 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax:925-798-1622 <br /> http://www.mccampbell.com E-mail:main@mccampbell.com <br /> Advanced GeoEnvironmentafDate Sampled: 04/22/98 <br /> Client Project ID: Stockton Plat <br /> Date Received: 04/24/98 . <br /> 4005 North Wilson Way <br /> Stockton,CA 95205 Client Contact:Bill Little Date Extracted: 04/24/98 <br /> Client P.O: Date Analyzed: 04/27-04/28/98 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 88428 <br /> Client ID AS136-55 <br /> Matrix S <br /> Compound Concentration' Compound Concentration* <br /> Acetone' ' ND<100 Ethylbenzene 200 <br /> Benzene 94 Hexachlorobutadiene ND<20 <br /> Bromobenzene ND<20 lodomethane ND<20 <br /> Bromochloromethane ND<20 lsopropylbenzene 25 ` <br /> Bromodichloromethane ND<20 p-Isopropyl toluene ND<20 <br /> Bromoform ND<20 Methyl butyl ketone' ' ND<20 <br /> Bromomethane NIX20 Methylene Chloride" ND<20 <br /> n-Butyl benzene 49 Methyl ethyl ketone" ND<20 <br /> sec-Butyl benzene ND<20 Methyl isobutyl ketone`s ND<20 <br /> ten-Butyl benzene 83 Methyl tert-Butyl Ether(MTBE) -- <br /> Carbon Disulfide ND<20 Naphthalene 53 <br /> Carbon Tetrachloride ND<20 n-Propyl benzene 110 <br /> Chlorobenzene ND40 Styrene' ' ND<20 <br /> Chloroethane ND<20 1,1,1,2-Tetrachloroethane ND<20 <br /> 2-Chloroethyl Vinyl Ether` ND<20 1,1,2,2-Tetrachloroethane ND<20 <br /> Chloroform ND<20 Tetrachloroethene ND<20 <br /> Chloromethane ND<20 Toluene 520 <br /> 2-Chlorotoluene ND<20 1,2,3-Trichl orobenzene ND<20 <br /> 4-Chlorotoluene ND<20 1,2,4-Trichlorobenzene ND<20 <br /> Dibromochloromethane ND<20 1,1,1-Trichloroethane ND<20 <br /> 1,2-Dibromo-3-chloropropane ND<20 1,1,2-Trichloroethane ND<20. <br /> Dibromomethane ND<20 Trichloroethene ND<20 <br /> 1,2-Dichlorobenzene ND<20 Trichlorofluoromethane ND<20 <br /> 1,3-Dichlorobenzene ND<20 1,2,3-Trichloropropane ND<20 <br /> 1,4-Dichlorobenzene ND<20 1,2,4-Trimethylbenzene 610 <br /> Dichlorodifluoromethane ND<20 1,3,5-Trimethylbenzene 220 " <br /> IJ-Dichloroethane ND<20 Vinyl Acetate <br /> 1,2-Dichloroethane ND<20 Vinyl Chloride"" ND<20 <br /> l,]-Dichloroethene ND<20 Xylenes,total '°' 1100 <br /> cis-1,2-Dichloroethene ND<20 <br /> trans-1 2-Dichloroelhene ND<20 <br /> 1,2-Dichloropropane ND<20 <br /> 1,3-Dichloropropane ND<20 <br /> 2,2-Dichloropropane ND<20 Comments: <br /> 1,1-Dichloropropene ND<20 Surrogate Recoveries(%) <br /> cis-1,3-Dichloropropene ND<20 Dibromofluoromethane 92 <br /> trans-l,3-Diehl oropropene ND<20 Toluene-dg 99 <br /> Ethylene dibromide ND<20 4-Bromofluorobenzene 109 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits uniess otherwise stated: water samples 1.0 ug/L; vapor samples 0.5 ug/L; solid and sludge samples 5 ug/kg; wipes <br /> 0.2uglwipe ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone; (h)lighter than water immiscible sheen is present; (i)liquid sample that contains greater than--5 vol. % <br /> sediment;0)sample diluted due to high organic content;(k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte;(1)methylbenzene;(m)acetic acid ethenyl ester;(n)chloroethene,(o)dimethylbenzenes. <br /> DHS Certification No. 1644 // Edward Hamilton,Lab Director <br /> i _ <br />