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i Ii(71nd Alenne tihuih #D7 Y'irheco C 4 94it3 »hll <br /> cC - – — --- <br /> le Y()A ampbell Analytical, Inc. ielep1mmir '1J] 79b-IbPU t`ax 921 198 Ib2_ <br /> 4VLbyitc www siK,Laumbell Lane I• u><kd mamolime nil out <br /> QC SUMMARY REPORT FOR SW8021B/8015Cm <br /> W O Sample Matrix Water QC Matrix Water Workorder 0602277 <br /> EPA Method SW80211318015Cm Extraction SW5030B BatchlD 20344 Spiked Sample ID 0602277-001A <br /> Analyte - Sample Spiked MS MSD T MS-MSD LCS LCSD LCS-LCSD Acceptance Catena (%) <br /> pg/L pglL % Rec l %Rec %RPD %Rec % Ree %RPD MS/MSC LCS 1 LCSD <br /> TPH(btex)e ND 60 103 113 _ 936 995 101- l 34 70 130 70- 130 <br /> MTBE ND 10 966 104 729 96 997 676 70- 130 70-130 <br /> BLncLnL ND l0 102 101 0 B89 999 101 1 16 70-130 70-130 <br /> ToltiLl ND 10 948 954 0 683 95 2 93 7 1 60 70-130 70-130 <br /> Ethylben2enc ND 10 MI 101 I 0 105 948 993 70- 110 70- 130 <br /> Xylenes ND 30 91 i 95 I 430 953 91 4 65 70- 110 70- 110 <br /> °/a5S 101 10 98 101 245 103 101 i 206 70- 130 70- 130 <br /> All l.(rgLt Lompounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions <br /> NON1- <br /> BATCH 20344 SUMMARY <br /> ample ID Date Sampled Date Extracted Date Analyzed Sample ID Date Sampled Date Extracted Date Analyzed <br /> 02277-001A 2115/06 1 00 PM 2116'06 2116106 11 15 1'M 0602277-002A 2115106 1 30 PM T21[7100 2(17,06 5 37 AM <br /> 0602277-003A 2/15106 1 40 PM 2/17/06 2/17/06409 AM <br /> MS=Matrix Spike,MSD=Matrix Spike Duplicate LCS=Laboratory Control Sample LCSD=Laboratory Control Sample Duplicate RPD=Relative Percent Deviation <br /> %Recovery=100'(MS-Sample)I(Amount Spiked) RFD=100'(MS- MSD)I((MS+MSD)12) <br /> MS 1 MSD spike recoveries and I or%RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons a)the sample is mhomogeneus AND <br /> contains significant concentrations of analyte relative to the amount spiked or b)the splked sample's matrix interferes with the spike recovery <br /> Z TPH(btex)=sum of BTEX areas from the FID <br /> #cluttered Chromatogram sample peak coelutes with surrogate peak <br /> =not applicable or not enough sample to perform matrix spike and matrix spike duplicate <br /> N R=anal a concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due?*high matrix or analyte content <br /> DHS Certification No 1644 QA/QC Officer <br />