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I <br /> M Lad AWAIM South 131 Natlicui ( A ()4513-,500 <br /> k c�"ampbell Analytical, 1��:�T TLICpi 92ti40-1r,2n F�Rn W» 19H tri), <br /> �3 W rhvie w W w Ina Licit l t nm I rttml 111nm a int eaniphell LOM <br /> • QC SUMMARY REPORT FOR SW8260B <br /> W 0 Sample Matnx Water QC Matnx Wates WorkOrder 0602277 <br /> EPA Method SW8260B Extraction SW5030B BatchlD 20341 Spiked Sample ID 0602277-001C <br /> Analyte Sample Spiked MS MSD MS-MSD LCS i llLCS_LCSD Acceptance Cntena(%) <br /> I <br /> pg1L pg/L % Rec %Rec %RPD %Rec % Rec %RPD INS 1 MSD LCS 1 LCSD <br /> i I � <br /> tett-Amyl methyl tthtr(TAME) ND 10 968 951 i 181 101 988 1 2 50 70 130 70- 130 <br /> t-Butjl alcohol(TBA) - ND 50 88 2 966 i 199 888877 893 0 430 70 t30 70- 130 <br /> Dusopiopyl ether(RIPE) ND 10 103 104 109 106 102 342 70-130 70- 130 <br /> Ethyl tort butyl ethtr(ETBL) ND Ill 97 3 97 6 0 359 101 98 6 225 70-130 70- 130 <br /> Methyl-t-butyl ether(M 1131-) ND 10 Y 954 100 488 996 989 0 767 70- 130 70-130 <br /> %951 105 10 104 101 I 137 100 100 0 70- 130 70- 130 <br /> All target compounds in the Method Blank of this extraction batch ut is ND less than the,method RL with the 10110wtng exttptions <br /> NONI- <br /> BATCH 2O341 SUMMARY <br /> Sample 10 Date Sampled Date Extracted Date Analyzed Sample ID tate Sampled Date Extracted Date Analyzed <br /> 0602277-001 C 2115/06 1 00 PM 2117106 2117106 2 43 AM 0602277-0028 2115/00 1 30 PM 2117106 21l T06 3 25 AM <br /> 02277-0038 2115106 1 40 PM 2117106 2117/06 4 07 AM <br /> MS=Matrix Spike MSD=Matrix Spike Duplicate LCS=Laboratory Control Sample LCSD=Laboratory Control Sample Duplicate RPD=Relative Percent Deviation <br /> %Recovery=100'(MS-Sample)I(Amount Spiked) RPD=100*(MS- MSU)I((MS+MSD)12) <br /> MS!MSD spike recoveries and I or%RPD may(ail outside of laboratory acceptance criteria due to one or more of the following reasons a)the sample is inhomogenous AND <br /> contains significant concentrations of analyte relative to the amount spiked or b)the spiked sample's matrix Interferes with the spike recovery <br /> N/A=not enough sample to perform matrix spike and matrix spike duplicate <br /> NR=analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyse content <br /> Ooratoryextraction solvents such as methylene chloride and acetone may occasionally a2pear in the method blank at low levels <br /> DHS Certification No 1644 QA/QC Officer <br />