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ni a1 <br /> tp <br /> I I U 2nd 16cnuc South un7 Pd[hlLO (n 94N53-5�)0 <br /> MeC ampbeli Analytical, Inc lelephmie 92>''981620 1.ir 925 Mh 1622 <br /> WLbsite NHw nrcampbell coin C mill iruinl mix�dinphell cont ^� <br /> QC SUMMARY REPORT FOR SW8021B/8015Cm <br /> W 0 Sample Matnx Water QC Matrix Water WorkOrder 0601215 <br /> EPA Method SW80216/8015Cm Extraction SW5030B Batchid 19885 Spiked Sample ID 0601213-004A <br /> Analyte Sample Spiked MS MSD MS-MSD LCS LCSD I LCS-LCSD Acceptance Cntena(%) <br /> pglL pglL %Rec , % Rec % RPD %Rec % Rec % RPD MS/MSD LCS/LCSD <br /> TPH(btcx)� ND 60 106 106 0 108 942 133 70- 130 70 130 <br /> MTBE ND 10 957 101 5 74 96 109 127 70-130 70- 130 <br /> fieniene ND 10 91 1 91 1 0 Y 946 927 206 70-1341 70- 130 <br /> Toluene W ND 10 92 7 } 907 210 962 93 1 320 70-130 70-130 <br /> Ethylbcnccne ND 10 93 5 I 94 0 599 98 942 400 70-130 70-130 <br /> Xylenes NI) 30 95 947 03S1. 997 95 479 70 130 1 70 130 <br /> %SS 101 10 99 97 126 99 99 0 70-130 70- 130 <br /> All talrzt compounds in the Method Blank ul this"traction batch were ND less than the method RL with the following exceptions <br /> NONE <br /> BATCH 19885 SUMMARY <br /> ample ID Date Sampled Date Extracted Date Analyzed Sample ID Dale Sampled Date Extracted Date Analyzed <br /> 01215 001A 1116/06 1 30 PM 1 18/06 ]r 18/06 900 PM 3 0601215-002A _ 1116106 l 40 PM 1119/06 1 19106 2 19 I'M <br /> 0601 2 1 5-003A 1/16/161 20 I'M It]9106 1/18/06959 PM <br /> MS=Matrix Spike,MSO=Matrix Spike Duplicate,LCS=Laboratory Control Sample LCSD=Laboratory Control Sample Duplicate,RPD=Relative Percent Deviation <br /> %Recovery=100'(MS Sample)/(Amount Spiked) RPD=100"(MS MSO)!((MS+MSD)12) <br /> MS 1 MSD spike recoveries and I or%RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons a)the sample is Inhornogenous AND <br /> contains significant concentrations of analyte relative to the amount spiked or b)the spiked sample s matrix Interferes with the spike recovery <br /> £TPH(btex)=sum of BTEX areas from the FID <br /> #cluttered chromatogram sample peak coal utes with surrogate peak <br /> ION=not applicable or not enough sample to perform matrlx spike and matnx spike duplicate <br /> NR=analyte concentration In sample exceeds spike amount for 5011 matrix or exceeds 2x s Ike amount for water matrix or sample diluted due to high matrix or analyte content <br /> DFIS Certification No 1644 QA/QC Officer <br />