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to k-nesapeaxe unve Kedwood Lity,(.A 94063 (415) 364 961Xl 4AX(41,51 364 9233 <br /> 404 N Wiget Lane Walnut Creek,CA 94598 (510) 988 9600 I•AX(510)988 9673 <br /> Analytical 819 Striker Avenue,Suite 8 Sacramento CA 95834 (916) 921 9600 FAX(916)921 0100 <br /> 1wround Zero Analysis, Inc Client Prolec6D 6215 Tam O'Shanter, Stockton <br />' 3422 West Hammer Lane, Ste C294 Matrix Solid <br /> Stockton, CA 95219 <br /> Attention John Lane Work Order# 9510J51-014 03 Reported Nov 7, 1995;, <br /> 4 <br /> v.i,., v S , N w1 , . l r n r r r r}m „ r t r A v , 4 r .. ,v, , ryr. ♦ n xr r r.r v +n, 41 v 4 r. v r . .u ,v r x v i n v r f <br />' QUALITY CONTROL DATA REPORT <br />' Analyte. Total Organic Total Igeldahl Phosphorous <br /> Carbon Nitrogen <br /> GC Batch#- IN1030959060TCA IN110295351400A IN110695365200A <br />' Analy Method. EPA 9060 EPA 351 4 EPA 365 2 <br /> Prep Method. N/A N/A N/A <br /> Analyst Y Arteaga Y Arteaga K Newberry <br />' MS/MSD #. 9510J5101 951OJ5101 951OJ5103 <br /> Sample Conc : 1700 370 240 <br /> Prepared Date- 10/30/95 11/2/95 11/6/95 <br />' Analyzed Date: 10/30/95 11/2/95 11/6/95 <br /> Instrument I D #' TOC1 Manual Manual <br /> Conc. Spiked 50000 mg/Kg 400 mg/Kg 500 mg/Kg <br />' Result 42000 3600 300 <br /> MS %Recovery 81 81 12 <br /> Dup Result, 46000 3500 290 <br /> MSD % Recov 89 78 10 <br /> RPD. 84 38 18 <br /> RPD Limit: 0-40 0-40 0-40 <br />' LCS #. LCS103095 LCS110295 LCS110695 <br /> Prepared Date: 10/30/95 11/2/95 11/6/95 <br />' Analyzed Date: 10/30/95 11/2/95 11/6/95 <br /> Instrument I D.#. TOC1 Manual Manual <br /> Cont; Spiked 200 mg/Kg 100 mg/Kg 0 50 mg/L <br />' LCS Result 2100 107 042 <br /> LCS% Recov 105 107 84 <br />' 60-140 60-140 60.140 <br /> LCS 80-120 80-120 80-120 <br /> Control Limits <br /> Please Note <br /> WProllect <br /> The LCS is a control sample of known,interferent-free matrix that is analyzed using the same reagents, <br /> NALYTICAL preparation,and analytical methods employed for the samples The matrix spoke is an aliquot of sample <br /> fortified with known quantities of specific compounds and subjected to the entire analytical procedure if <br /> the recovery of analytes from the matrix spike does not fall within specified control limits due to matrix <br /> interference,the LCS recovery is to be used to validate the batch <br /> er <br /> ager **MS=Matrix Spike,MSD=MS Duplicate, RPD=Relative 96 Difference 9510J51 GGG <2> <br />