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FRIKIM (CES ON <br /> GHw0 GAO = U rCH CERTIFICATE OF ANALYSIS <br /> Ana/ytica/ Laboratory <br /> Monday, November 01, 1999 <br /> TO: William Little <br /> Advanced GeoEnvironmental, <br /> 4005 N. Wilson Way <br /> Stockton, Ca. 95205 <br /> t, <br /> Sample Information <br /> Sample ID: PE6245- 15 Sample Type: Grab <br /> Description:im <br /> Sample DescrD 6 <br /> p P � Project Name: Quick & Save 1901 So, Eldo <br /> Date/Tinte Sampled: 10/21 /99 12:25:00 PM Sample Matrix: Soil <br /> ANALYTICAL RESULT QA/QCREPORT <br /> Dare LCS Spike MS Spike <br /> }. ,. Test Parameter Method DLR Unit Resrdt Analyzed Blank Colic, LCS% Colic. MS% MSD RSD <br /> t: i Lead (Pb) EPA 6010 1 mg/Kg 7 01 -Nov-99 No 0.02 91 .6% 0.02 114.4% 118.0% 0.8% <br /> TPH-Gasoline EPA 8015M/DHS 1 mg/Kg ND 25-Oct-99 NO 0.5 96.0% 0.5 102.0% 90.0% 3.1 % <br /> TPH-Diesel EPA8015M/DHS 1 mg/Kg ND 25-Oct-99 NO 50 96.0% 50 110.0% 104.0% 1 .4% <br /> Methyl t-Butyl Ether (MtBE) EPA8260 5 ug/Kg 16.0 25-Oct-99 ND 40 87.5% 40 87.5% 105.0% 4.5% <br /> ' 1 <br /> Diisopropyl ether (DIPE) EPA8260 ^ 5 ug/Kg ND 25-Oct-99 NO 40 95.0% 40 95.0% 97.5% 0.6% <br /> 4 Ethyl-t-butyl ether (ETBE) EPA8260 5 ug/Kg ND 25-Oct-99 NO 40 90,0% 40 90.0% 97.5% 2.0% <br /> Tert-amyl methyl ether (TAME) EPA8260 5 ug/Kg NO 25-Oct-99 NO 40 100.0% 40 105.0% 102.5% 0.6% <br /> t-Butanol (TBA) EPA8260 5 ug/Kg NO 25-Oct-99 ND 40 87.5% 40 87.5% 85.0% 0.7% <br /> Benzene EPA 8260 5 ug/Kg ND 25-Oct-99 ND 40 95.0% 40 137.5% 140.0% 0.5% <br /> Toluene EPA 8260 5 ug/Kg ND 25-Oct-99 ND 40 95.0% 40 120.0% 130.0% 2.0% <br /> IL <br /> Ethyl Benzene EPA 8260 5 ug/Kg ND 25-Oct-99 ND 40 87.5% 40 102.5% 120.0% 3.9% <br /> Xylene, Total EPA 8260 5 ug/Kg NO 25-Oct-99 ND 80 93.80/6 80 143.80/6 156.3% 2.1 <br /> rngeT = ntlligeoms per Liter = ppm DLR- Detection l imi/for the Purpose of Reporting. RSD- represent relative percent di((erent (RPD) between duplicates spike ofsaorples <br /> It <br /> ugiL - nocrogromr per Liter = ppb Grceplional sample rnalvices or inter(erenece.s rnoy result in or Duplicate nfSample <br /> C - Composite G �= Grob higher detection limits AIS/MSD nieasure of the percent recover), e((rcnencies wilhin the nunris <br /> i <br /> LCS- measure of the percent recovery a/the Laboratory Control Spike (1_CS) <br /> K'.. , RESpE T UL4�TED, <br /> t� <br /> JwathanHaloV. Le, Laboratory Director <br /> EPA-Envirmunemtd Pi ofection Agency Method. Page I of t <br /> .1'll-,Ctnrrrlrrrdit if,llrnd lar Fr.amnper rit) r,.,r, a51mr I Yn inti , n.,r. I.Pt. "I n . . . � . n r. � _ _ r . . . . _ n . .� . .. .N r . .. ., -. .. �. � <br />