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Alpha Analytical, Inc. <br /> 255 Glendale Ave. • Suite 21 •Sparks,Nevada 89431-5778 <br /> (775)355-1044 •(775)355-0406 FAX• 1-800-283-1183 <br /> Dale: Q ma C Summary Report Work Order: <br /> 06-Mar-14 p 14022702 <br /> Method Blank Type MBLK Test Code: EPA Method SW8260B <br /> File ID 14022805.D Batch ID:MS12WO228A Analysis Date: 02128/2014 12:57 <br /> Sample ID: MBLK MS12WO228A Units: yg/L Run ID:MSD-12-140228A Prep Date: 02/28/2014 12:57 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME) RPDRefVal %RPD(Limit) Qual <br /> Tertiary Butyl Alcohol(TBA) ND 10 <br /> Methyl tert-butyl ether(MTBE) ND 05 <br /> Dkisopropyl Ether(DIPE) ND 1 <br /> Ethyl Tertiary Butyl Ether(ETRE) ND 1 <br /> 1,2-Dichloroethane ND 1 <br /> Benzene ND 0.5 <br /> Tertiary Amyl Methyl Ether(TAME) ND 1 <br /> Toluene ND 0.5 <br /> 1,2-Dibromoethane(EDB) ND 2 <br /> Ethylbenzene ND 0.5 <br /> m,p-Xylene ND 0.5 <br /> o-Xylene ND 0.5 <br /> Surr: 1,2-Dichloroethane-d4 11.7 10 117 70 130 <br /> Surr:Toluene-d8 10.3 10 103 70 130 <br /> Surr:4-Bromofluorobenzene 9.14 10 91 70 130 <br /> Laboratory Control Spike Type LCS Test Code: EPA Method SW8260B <br /> File ID: 14022804.13 Batch ID: MS12WO228A Analysis Date: 02/28/2014 12:21 <br /> Sample ID: LCS MS12WO228A Units : Ng/L Run 10:MSD_12 140228A Prep Date: 02128/2014 12:21 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME)RPDRefVal %RPD(Limit) Qual <br /> Methyl tert-butyl ether(MTBE) 7.95 0.5 10 80 63 137 <br /> Benzene 7.26 0.5 10 73 70 130 <br /> Toluene 8.45 0.5 10 85 80 120 <br /> Ethylbenzene 8.47 0.5 10 85 80 120 <br /> m,p-Xylene 8.54 0.5 10 85 65 139 <br /> o-Xylene 8.36 0.5 10 84 70 130 <br /> Surr. 1,2-Dichloroethane-04 11.2 10 112 70 130 <br /> Surr:Toluene-08 10.1 10 101 70 130 <br /> Surr.4-Bromofluorobenzene 10 10 100 70 130 <br /> Sample Matrix Spike Type MS Test Code: EPA Method SW8260B <br /> File ID: 14022815.D Batch ID: MS12WO228A Analysis Date: 02128/2014 16:30 <br /> Sample ID 14022702-08AMS Units. pg/L Run ID:MSD_12_140228A Prep Date: 02/2812014 16:30 <br /> Analyte Result PQL SpkVal SpkRefVel %REC LCL(ME) UCL(ME)RPDRefVel %RPD(Limit) Qual <br /> Methyl tert-butyl ether(MTBE) 57.9 1.3 50 0 116 56 140 <br /> Benzene 42.2 1.3 50 0 64 67 134 <br /> Toluene 46.3 1.3 50 0 93 38 130 <br /> Ethylbenzene 45.9 1.3 50 0 92 70 130 <br /> m,p-Xylene 45.4 1.3 50 0 91 65 139 <br /> o-Xylene 45.9 1.3 50 0 92 69 130 <br /> Surr: 1,2-Dichloroethane-d4 60 50 120 70 130 <br /> Surr:Toluene-d8 49 50 98 70 130 <br /> Surr.4-Bromofluorobenzene 47.1 50 94 70 130 <br /> Sample Matrix Spike Duplicate Type MSD Test Code: EPA Method SW8260B <br /> File ID: 14022816.D Batch ID:MS12WO228A Analysis Date: 02/28/2014 16:51 <br /> Sample ID: 14022702-08AMSD Units: Ng/L Run ID:MSD-12-140228A Prep Date. 02128/2014 16:51 <br /> Analyte Result PQL SpkVal SpkReNal %REC LCL(ME) UCL(ME)RPDReNal %RPD(Limd) Qual <br /> Methyl tert-butyl ether(MTBE) 57.4 1.3 50 0 115 56 140 57.9 0.8(40) <br /> Benzene 47.2 1.3 50 0 94 67 134 42.17 11.3(21) <br /> Toluene 51.2 1.3 50 0 102 38 130 46.31 10.1(20) <br /> Ethylbenzene 51.5 1.3 50 0 103 70 130 45.87 11.6(20) <br /> m,p-Xylene 50.6 1.3 50 0 101 65 139 45.4 10.9(20) <br /> o-Xylene 51.5 1.3 50 0 103 69 130 45.91 11.5(20) <br /> Surr 1,2-Dichloroethane-d4 59.5 50 119 70 130 <br /> Surr:Toluene-d8 48.5 50 97 70 130 <br /> Surr.4-Bromofluorobenzene 47.6 50 95 70 130 <br />