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GeoAnalytical Laboratories, Inc. <br /> 2300 Maryann Dr. Turlock, CA 95380 Phone (209) 669-0100 Fax (209) 668-8516 <br /> email: lah.geo@att.net <br /> Report # WOJ0706 Project: 8th & Eldorado Stockton Date: 10/ 14/ 10 <br /> Jim Thorpe, Inc. Date Reed: 10/07/ 10 <br /> PO Box 357 <br /> Lodi, CA 95241 <br /> CERTIFICATE OF ANALYSIS <br /> Sampler: Richard Chrun <br /> Sample ID: TK- 1000 N W at 9' <br /> Lab ID Sample Date/ Time RL Method Analyte Result units Notes Started <br /> W010706-19 10/07/2010 14' 15 5.0 8260B 12-Dichloroetliane ND ug/kg 10/11/10 10: 19 <br /> 5.0 Benzene ND ug1kg <br /> 10.0 Di-isopropyl Ether (DIPE) ND ug/kg <br /> 400 Ethanol ND ug/kg <br /> 10.0 Ethyl len-Butyl Ethcr (ETBE) ND ug/kg <br /> 5.0 Ethylbenzene ND ug/kg <br /> 10.0 Ethylene dibromide ND ug/kg <br /> 10.0 Methyl ten-Butyl Ether (MTBE) ND ug/kg <br /> 10.0 Ten-Amyl Methyl Elhcr(TAME) ND ug/kg <br /> 200 ten-Butanol (TBA) ND ug/kg <br /> 5.0 Toluene ND ug/kg <br /> 5.0 Xylenes. total ND ug/kg <br /> 1 .0 GUMS Gasoline ND mg/kg <br /> Surrogate Amnt Spiked Arrant Recovered % Recovery QCLimit % Surrogate Notes <br /> 1 ,2-DichlomethaneA41 20.00 22.2 111 % 72-132 <br /> 2-Bromo- I -Chloropropane 20.00 24.7 124 % 71-134 <br /> 4-Bramolluombemene 20.00 16.5 83 % 74-132 <br /> Sample ID: TK- 1000 NE at 9' <br /> Lab ID Sample Date/ Time RL Method Analyte Result Units Notes Started <br /> W010706-20 10/072010 14' 18 1250 8260B 1 ,2-Dichlorocthane ND ug/kg 10/11 / 10 10: 19 <br /> 1250 Benzene ND ug/kg <br /> 2500 Di-isopropyl Ether (DIPE) ND ug/kg <br /> 100000 Ethanol ND ug/kg <br /> 2500 Ethyl tort-Butyl Ether (ETBE) ND ug/kg <br /> 1250 Ethylbenzene 27600 ug/kg F <br /> 2500 Ethylene dibromide ND ug/kg <br /> 2500 Methyl ten-Butyl Ether (MTBE) ND ug/kg <br /> 2500 Ten-Amyl Methyl Ether(TAMF.) ND ug/kg <br /> 50000 ten-Butanol (TBA) ND ug/kg <br /> 1250 Toluene 7520 ug/kg - <br /> 1250 Xylenes, total 163000 ug/kg <br /> 250 GC/MS Gasoline 1930 mg/kg D-26 <br /> Surrogate Amnt Spiked Amur Recovered % Recovery QC Limit % SurrogateNotes <br /> 1 ,2-Dichloroethanc-d4 5000 4450 89 % 71-132. <br /> 2-Bmmo-I -Chloroprepane 5000 4550 91 % 71-134 <br /> 4-BromoOuorobenzene 5000 5200 104 % 74-131 <br /> Certification # 2585 <br />