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Entech Analytical Labs, Inc , Santa Clara, CA <br />' Lab Report No H2O22801 Date 03/06/2002 Page 8 <br /> Protect Name VALENTINE Analysis Volatile Organic Compounds by GC/MS Fuel <br /> Project No 7232 Method 8260FA <br /> Prep Meth SW5030B <br />' Field ID MW-6 Lab Samp ID 29086-003 <br /> Descr/Location MW-6 Recd Date 02/28/2002 <br /> Sample Date 02/27/2002 Prep Date 03/01/2002 <br /> Sample Time 1018 Analysis Date 03/01/2002 <br /> Matrix Water QC Batch WMS31450 <br /> Basis Not Filtered Notes BH <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Dal <br /> Methyl-tort-butyl ether (MTBE) 3 50 PQL ND UGIL 10 <br />' tert-Butyl ethyl ether(ETBE) 5 50 PQL ND UG/L. 10 <br /> tert-Amyl methyl ether(TAME) 3 50 PQL ND UGIL 10 <br /> Di-isopropyl ether(D1PE) 5 50 PQL ND UGIL 10 <br />' tert-Butyl alcohol (TBA) 110 200 PQL ND LIG/L. 10 <br /> 1,2-Dichloroethane 3 50 PQL ND UGIL 10 <br /> 1,2-Dibrornoethane 5 50 PQL ND UGIL 10 <br /> ' SURROGATE AND INTERNAL STANDARD RECOVERIES <br /> 4-Bromofluorobenzene 65-135 SMSA 85% 1 <br /> Toluene-d8 77-150 SMEA 109% 1 <br /> Dibromofluoromethane 57-156 SMSA 98% 1 <br /> BH Reporting limits raised due to high level of non-target analytes <br /> 1 <br /> I <br /> 1 <br /> Approvea ny nate <br />