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Entech Analytical Labs, Inc , Santa Clara, CA <br /> Lab Report No H2O22801 Date 03/06/2002 Page 1 <br /> ' Project Name VALENTINE Analysis Volatile Organic Compounds by GC/MS Fuel <br /> Project No 7232 Method 8260FA <br /> Prep Meth SW5030B <br /> ' Field ID MW-1 Lab Samp ID 29086-005 <br /> Descr/Location MW-1 Recd Date 02/28/2002 <br /> I Sample Date 02/27/2002 Prep Date 03/01/2002 <br /> Sample Time 1127 Analysis Date 03/01/2002 <br /> Matrix Water QC Batch WMS31450 <br /> ' Basis Not Filtered Notes <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tent-butyl ether(MTBE) 03 5 PQL ND UG/L 1 <br /> tent-Butyl ethyl ether(ETBE) 05 5 PQL ND UG/L 1 <br /> tert-Arnyl methyl ether(TAME) 03 5 PQL ND UG/L 1 <br /> Di-isopropyl ether(D1PE) 05 5 PQL ND UG/L 1 <br /> ' tert-Butyl alcohol (TBA) 11 20 PQL ND UG/L 1 <br /> 1,2-Dichloroethane 03 5 PQL ND UGIL 1 <br /> 1,2-Dibromoethane 05 5 PQL ND UGIL 1 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES <br /> 4-Bromofluorobenzene 65-135 SMEA 86% 1 <br /> Toluene-d8 77-150 SMEA 105% 1 <br /> Dibromofluoromethane 57-156 SMSA 98% 1 <br /> i <br /> Approvea Dy -, vate l2 b 7i <br /> r <br />