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Entech Analytical Labs, Inc , Santa Clara, CA <br /> 1 Lab Report No H2022801 Date 03/06/2002 Page 3 <br /> ' Project Name VALENTINE Analysis Volatile Organic Compounds by GC/MS Fuel <br /> Protect No 7232 Method 8260FA <br /> Prep Meth SW50308 <br /> ' Field ID MW-2 Lab Samp ID 29086-008 <br /> Descr/Location MW-2 Rec'd Date 02128{2002 <br /> Sample Date 02/27/2002 Prep Date 03/02/2002 <br /> Sample Time 1310 Analysis Date 03/02/2002 <br /> Matrix Water QC Batch WMS31450 <br /> Bans Not Filtered Notes BH <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tert-butyl ether(MTBE) 30 500 PQL ND UG/L 100 <br /> tert-Butyl ethyl ether(ETRE) 50 500 PQL ND UG/L 100 <br /> tert-Amyl methyl ether(TAME) 30 500 PQL ND UG/L 100 <br /> Di-isopropyl ether(DIPE) 50 500 PQL ND UG/L 100 <br /> ' tert-Butyl alcohol (TBA) 1100 2000 PQL ND UG/L 100 <br /> 1,2-Dichloroethane 30 500 PQL ND UG/L 100 <br /> 1,2-Dibromoethane 50 500 PQL ND UG/L 100 <br /> ' SURROGATE AND INTERNAL STANDARD RECOVERIES <br /> 4-Bromoflu o ro benzene 65-135 SMEA 84% 1 <br /> Toluene-d8 77-150 SMSA 108% 1 <br /> Dibromofluoromethane 57-156 SMEA 100% 1 <br /> BH Reporting limits raised due to high level of non-target analytes <br /> 1 <br /> Approvea Dy uate �7 �� <br />