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i <br /> i <br /> Analytical Lnhot atory ��of 5s <br /> CERTIFICATE OF ANALYSIS <br /> Friday June 23 2006 <br /> Attention Jack Bishop <br /> California Tank Lines Report Page 18 of21 <br /> P O BOX 6245 <br /> Stockton, CA 95206 <br /> Volatile Organic Compounds by EPA Method 8260B-Quality Control <br /> Precision Envlro-Tech <br /> i <br /> Reporting Spike Source % EC RPP <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch AD60101-Volatiles <br /> I <br /> Blank(AD60101-BLKI) Prepared 31-Mar-06 Analyzed 01-Apr-06 <br /> tert Butyl Aeohol(TBA) ND 500 ug/1 <br /> Methyl tert butyl Ether(MtBE) ND 0 500 <br /> Dnsopropyl Ether(DWE) ND 0 500 <br /> Ethyl tert Butyl Ether(ETBE) ND 0 500 <br /> tert Amy]Methyl Ether(TAME) ND 0 500 <br /> 1 2 Dibromoethme(EDB) ND 0 500 <br /> 12 Dicbloroethane ND 100 <br /> Benzene ND 0 500 <br /> Ethylbenzene ND 0 500 <br /> Toluene ND 0 500 <br /> 4 Xylene ND 1 00 <br /> ylene ND 100 <br /> LCS(AD60101-BSI) Prepared 31-Mar-06 Analyzed 01-Apr-06 <br /> Benzene 159 0 500 ug11 200 80 75 122 <br /> Ethylbenzene 162 0 500 200 81 75 122 <br /> Toluene 160 0 500 200 so 75 122 <br /> in p Xylene 42 0 100 400 105 75 122 <br /> o-Xylene 230 100 200 115 75 122 <br /> Matrix Spike(AD6010I-MSI) Source 6033007-01 Prepared 31-Mar-06 Analyzed 01-Apr 06 <br /> Benzene 159 0 500 ug/l 200 ND 80 75 125 <br /> Ethylbenzene 18 0 0 500 200 ND 90 75 125 <br /> Toluene 212 0 500 200 ND 106 75 125 <br /> m p-Xylene 35 8 100 400 ND 90 75 125 <br /> o Xylene 224 1 00 200 ND 112 75 125 <br /> Matrix Spike Dup(AD60101-MSDI) Source 6033007-01 Prepared 31-Mar 06 Analyzed 01-Apr-06 <br /> Benzene 193 0 500 ugfi 200 ND 92 75 125 14 20 <br /> Ethylbenzene 205 0 500 200 ND 102 75 125 13 20 <br /> Toluene 196 0 500 200 ND 98 75-125 8 20 <br /> m p-Xylene 354 100 400 ND 88 75 125 l 20 <br /> o-Xylene 23 1 100 200 ND 116 75 125 3 20 <br /> mg I=milhgmms per Laer ppm DI R !>erecrron Lrmrr furl nrpose nfRermm�R <br /> reg L=micrograms per Liter=ppb h rceplroml crumple marrnces or inierferem n may <br /> resuir m hrghrr derecaan hnia, <br /> RESPECTFULLY SUBMITTED, <br /> *(:��/Ot'z� <br /> Jonathan Le,Laboratory Director <br /> %-{.1 % it est Lane �u1fe B2 Slotklon C 4 95210 nhone (209 4 7-8105 T ct� 1ZU91 4,77-.S 1�tS <br />