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110 2nd Avenue South,#137,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> 20 http//www mecampbell co m E-mail main@mccampbell com <br /> ' Advanced GeoEnvironmental Client Project ID Pacific Pride S El Date Sampled 03/01/2002 <br /> Dorado Date Received 03/05/2002 <br /> 837 Shaw Road <br /> ' Stockton, CA 95215 Chent Contact Tian Cuellar Date Extracted 03/05-03/07/2002 <br /> Chent P O Date Analyzed 03/05-03/07/2002 <br /> ' Seven Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab ID 0203071- 0203071- 0203071- <br /> 005 006 007 Reporting Lirrut <br /> Client ID MW5/03010 MW6/03010 MW7/03010 <br /> 2 2 2 <br /> ' Matrix W W W S W <br /> Compound Concentration* ug/kg ug/L <br /> ' Di-isopropyl Ether(DIPE) ND ND " ND<50 50 10 <br /> ' Ethyl tent-Butyl Ether(ETRE) ND ND ND<50 50 10 <br /> Methyl tert-Butyl Ether(MTBE) ND 1 1 ND<50 50 to <br /> tert-Amyl Methyl Ether('TAME) ND ND ND<50 50 10 <br /> ' tert-Butanol ND ND ND<250 25 50 <br /> ' Methanol ND ND ND<25,000 2500 500 <br /> Ethanol ND ND ND<2500 250 50 <br /> 1 <br /> Surrogate Recaveries <br /> ' Dibromofluoromethane 110 112 105 <br /> ' Comments <br /> 'water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP I STLC I SPLP extracts in ug/L <br /> ' ND means not detected above the reporting limit,N/A means surrogate not applicable to flus analysis <br /> (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than—5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> 1 <br /> DHS Certification No 1544 Jk_Edward Hamilton,Lab Director <br /> I <br />