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COLUMBIA ANALYTICAL SERVICES,INC <br /> Analytical REport <br /> iClient ARCO Products Compan` Service Request. 59701961 <br /> ProleLt 20805 114 0081TO420791 0012130 STOCKTON Date Collected 9/30197 <br /> Semple M.striv Air Date Received. 10/1/97 <br /> BTCX and Total Volatile Hydrocarbons <br /> Sample Nam(, EFFLUENT Ututs PpmV <br /> Lab Code 59701961-002 Basis NA <br /> Test Notes <br /> Prep AnAvsis Dilution Date Date Result <br /> Andlvte Method Method VIRL Factor Extracted Analyzed Result Notes <br /> Benzene 5030 8020 01 1 NA 10/1/97 ND <br /> Toluene 5030 8020 0 1 1 NA 10/1/97 06 <br /> Ethylbenzene 5030 8020 0 1 1 NA 10/1/97 04 <br /> Xylenes Total 5030 8020 02 1 NA l0/1/97 15 <br /> Total Volatile Hvdrmarbons <br /> C, - <br /> I -CS 5030 8015M 5 1 NA 10/1/97 8 <br /> C6•C12 X030 8015M 5 l NA 10/1/97 83 <br /> TPH as Gasoline* 5030 9015M 5 1 NA 10/1/97 83 <br /> * TPH as gasoline is defined as C6(benzene)through C 12(dodecane)and uses a <br /> molecular weight of 100 to calculate the ppmv <br /> 1522/0205971) <br /> Page 6 <br />