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COLUMBIA ANALYTICAL SERVICES,INC. <br /> Analytical Report <br /> Client: EMCON Service Request: S9602044 <br /> Protect 2130 Stockton/#!21775-229 002/TO419350 00 Date Collected: 11/26/96 <br /> Sample Matrix Water Date Received: 1213196 <br /> Date Extracted- NA <br /> BTEX MTBE and TPH as Gasoline <br /> EPA Methods 5030/8020/California DHS LUFT Method <br /> Units ug/L(ppb) <br /> Sample Name MW-4 (74) MW-5(76) MW-6 (72) <br /> Lab Code 59602044-004 S9602044-005 S9602044-00- <br /> Date Analyzed 1216196 1216196 12/6196 <br /> Anahte MRL <br /> TPH as Gasoline 50 ND <200 X <200 X <br /> Benzene 05 ND 1 9 ND <br /> Toluene 05 ND ND ND <br /> Ethvlbenzene 05 ND 05 ND <br /> Total Xvienes 05 ND ND ND <br /> Methvl Cert-Butyl Ether 3 ND <4 D <4 D <br /> D The MRL is elevated because of matrix interferences <br /> X The sample contains non-fuel components eluting in the gasoline range and quantitated as <br /> gasoline The chromatogram does not match the typical gasoline fingerprint <br /> 3=060194 <br /> Page 4 <br />