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COLUMBIA ANALYTICAL SERVICES,INC. <br /> QA/QC Report <br /> Client EMCON Service Request S9602044 <br /> Protect 2130 Stockton/#21775-229 002/TO#19350 00 Date Collected. 11/26/96 <br /> Sample Matrix: Water Date Received- 12/3/96 <br /> Date Extracted NA <br /> Date Analvzed: NA <br /> Surrogate Recovery Summary <br /> BTEX,MTBE and TPH as Gasolme <br /> EPA Methods 5030/8020/California DHS L1JFT Method <br /> PID Detector FID Detector <br /> Percent Recovery Percent Recovery <br /> Sample Name Lab Code 4-BromotluorobenzenL a,a,cc—Fnfluorotoluene <br /> MW-1 (74) 59602044-001 95 106 <br /> MW-2 (72) 59602044-002 90 112 <br /> MW-3 (73) 59602044-003 104 100 <br /> MW-4(74) S9602044-004 101 97 <br /> MW-5(76) S9602044-005 102 96 <br /> MW-6(72) S9602044-006 99 106 <br /> MW-7 (72) 59602044-007 105 98 <br /> MW-10(7 1) S9602044-008 95 113 <br /> MW-7 (72) (MS) 59602044-007MS 101 108 <br /> MW-7 (72)(DMS) S9602044-007DMS 102 99 <br /> Method Blank 5961205-WB1 102 100 <br /> Method Blank S961206-WB1 102 96 <br /> CAS A4ceptance Limits 69-116 69-116 <br /> SUp,V060194 <br /> Page 8 <br />