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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax: 925-798-1622 <br /> http:/Iwww.mccampbell.com E-mail:main@mccampbell.com <br /> Advanced GeoEnvironmental Client Project ID:J.B.Murphy Trucking Date Sampled: 07/13/2000 <br /> 4005 North Wilson Way Date Received: 07/14/2000 <br /> Stockton,CA 95205 Client Contact:Brian Millman Date Extracted: 07/14/2000 <br /> Client P.O: Date Analyzed: 07/14-07/21/2000 <br /> Diesel Range(C10-C23)Extractable Hydrocarbons as Diesel <br /> EPA methods modified 8015,and 3550 or 3510;California RWQCB(SF Bay Region)method GCFID(3550)or GCFID(3510) <br /> Lab ID Client ID Matrix TPH(d)- %Recovery <br /> Surrogate <br /> 42959 P2-H2O W 2,100,000,a,h,i 116 <br /> 42960 P3-H2O W 21,000,a/e,i 99 <br /> 42961 P4-H2O W 2,900,000,a,h,i 100 <br /> 42962 P5-H2O W 3100,a,i 117 <br /> 42963 P6-H2O W 2200,g,i 117 <br /> } <br /> 42964 P7-H20 W 15,000,a,i 111 <br /> 42965 P8-H20 W 530,g,i Ill <br /> Reporting Limit unless otherwise W 50 u g/L <br /> stated;ND means not detected above <br /> the reporting limit S 1.0 mg/kg <br /> water and vapor samples are reported in ug/L,wipe samples in ug/wipe,soil and sludge samples in mg/kg,and all TCLP/STLC/SPLP <br /> extracts in ug/L <br /> N cluttered chromatogram resulting in coeluted surrogate and sample peaks,or;surrogate peak is on elevated baseline,or;surrogate has been <br /> diminished by dilution of original extract. <br /> 'The following descriptions of the TPH chromatogram are cursory in nature and McCampbell Analytical is not responsible for their <br /> interpretation:a)unmodified or weakly modified diesel is significant;b)diesel range compounds are significant;no recognizable pattern;c) <br /> aged diesel?is significant);d)gasoline range compounds are significant;e)medium boiling point pattern that does not match diesel(fuel <br /> oil?);f)one to a few isolated peaks present;g)oil range compounds are significant;h)lighter than water immiscible sheen is present;i) <br /> liquid sample that contains greater than—5 vol.%sediment. <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br />