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110 2nd Avenue South,4D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax: 925-798-1622 <br /> http:l/www.mccampbell.com E-mail:main@mccampbell.com <br /> l <br /> Advanced GeoEnvironmental Client Project ID:J.B.Murphy Trucking Date Sampled: 07/13/2000 <br /> 4005 North Wilson Way Date Received: 07/14/2000 <br /> Stockton, CA 95205 Client Contact:Brian Millman Date Extracted: 07114-0711812000 <br /> Client P.O: Date Analyzed: 07114-0711812000 <br /> •I Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab ID 42957 42958 42959 42960 <br /> Reporting Limit <br /> Client 1D P8-20 P1-H20 P2-H2O P3-H20 <br /> Matrix S W W W S w <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(DIPE) ND ND ND ND 5.0 1.0 <br /> Ethyl tert-Butyl Ether(ETBE) ND ND ND ND 5.0 1.0 <br /> Methyl-tert Butyl Ether(MTBE) ND ND ND ND 5.0 1.0 <br /> tent-Amyl Methyl Ether(TAME) ND ND ND ND 5.0 1.0 <br /> ,. tert-Butanol ND ND ND ND 25 5.0 <br /> Surrogate Recoveries(%) <br /> Dibromofluoromethane 109 87 114 111 <br /> Comments: h,i h,i i <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit;NIA means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present;(i)liquid sample that contains greater than—5 vol.%sediment;0)sample diluted due to <br /> high organic content <br /> DHS Certification No. 1644Edward Hamilton,Lab Director <br />