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3 <br /> 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAWBELL ANALYTICAL INC. Telephone:925-798-1620 Fax:925-798-1622 <br /> http://www.mccampbell.com E-mail:main@mecampbell.com <br /> Advanced GeoEnvironmental Client Project ID:J.B.Murphy Trucking Date Sampled: 07/13/2000 <br /> 4005 North Wilson Way Date Received: 07/14/2000 <br /> Stockton, CA 95205 Client Contact:Brian Millman Date Extracted: 07/14-07118/2000 <br /> Client P.O: Date Analyzed:07114-07118/2000 <br /> Oxygenated Volatile Organics By GUMS__ <br /> EPA method 8260 modified <br /> Lab ID 42965 <br /> LReporting Limit <br /> Client 1D P8-HZ0 <br /> Matrix W S W <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(DIPS) ND 5.0 1.0 <br /> Ethyl tert-Butyl Ether(ETBE) ND 5.0 1.0 <br /> ll :. Methyl-tert Butyl Ether(MTBE) ND 5.0 1.0 <br /> tert-Amyl Methyl Ether(TAME) ND 5.0 1.0 <br /> tert-Butanol ND 25 5.0 <br /> Surrogate Recoveries(%) <br /> Dibramotluoromethane 114 <br /> Comments: F <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L. <br /> ND means not detected above the reporting limit;NIA means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present;(i)liquid sample that contains greater than--5 vol.%sediment;0)sample diluted due to <br /> high organic content <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br />