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GeoAnalytical Laboratories, Inc. <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone (209)572-0900 Fax(209)572-0916 <br /> CERTIFICATE OF ANALYSIS <br /> Report# K055-09 Oxygenates Date: 3/7/99 <br /> Thorpe OilDate Rec'd: 2/24/99 <br /> PO Box 357 Project: Card-Lock Stockton (Alpine &West Lane) Date Started: 3/1/99 <br /> Date Completed: 3/1/99 <br /> Lodi CA 95241-0357 <br /> PO# Date Sampled: 2/24/99 <br /> Time: <br /> Sampler: RAzevedo(Geo) <br /> Sample ID: TK2-N/W @ 15' <br /> Lab ID: K20658 <br /> Method MDL Analyte Results Units <br /> 8260 250 Methyl tertiary-Butyl Ether (MTBE) 3500 pg/Kg ' <br /> 250 Ethanol ND pg/Kg <br /> 2500 tertiary-Butanol ND pg/Kg <br /> 250 Di-isopropyl ether (DIPE) ND pg/Kg <br /> 5030/LUFT 250 Ethyl tertiary-Butyl Ether (ETBE) ND pg/Kg <br /> 250 tertiary-Amyl Methyl Ether (TAME) ND pg/Kg <br /> Detection7iaKrenn <br /> ted due to presence of heavier hydrocarbons <br /> Donna Keller <br /> Chemist Certification # 1157 Laboratory Director <br />