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CASTLE ANALYTICAL LABORATORY <br />' Environmental Testing Services 2333 Shuttle Drive,Atwater, CA 95301 Phone (209)384-2930 <br /> Certificate No 2480 Fax (209)384-1507 <br /> Advanced GeoEnvironmental Inc Client Project ID Pacific Pride-West Lane Sampled 10-09-03 <br />' of Northern California Reference Number 6211 Received 10-14-03 <br /> 837 Shaw Road Sample Description Water Extracted 10-19-03 <br /> Stockton, CA 95215 Sample Prep/Analysis Method EPA 5030/8260 Analyzed 10-19-03 <br /> Attn Tim Cuellar Lab Numbers 6211-12W Reported 10-30-03 <br /> GASOLINE ADDITIVES AND SOLVENTS BY EPA METHOD 8260 GC/MS <br /> ANALYTE REPORTING SAMPLE ID <br /> I LIMIT P9 <br /> 65 to 68 <br /> (p IL) (u IL) <br /> FUEL OXYGENATES <br /> Methyl tert-Butyl Ether(MTBE) 050 059 <br /> Di-isopropyl Ether (DIPE) 0 50 ND <br /> Ethyl tert-Butyl Ether (ETBE) 050 ND <br /> tert-Amy!Methyl Ether(TAME) 1150 ND <br />' tert-Butanol(TBA) 20 ND <br /> VOLATILE HALOCARBONS <br /> 1 2-Dichloroethane (1 2-DCA) 050 12 <br /> Ethylene Dibromide (EDB) 050 ND <br /> Report Limit Multiplication Factor 1 <br /> I <br /> Surrogate Recoveries <br /> I 1 2-Dichloroethane-d4 104% <br /> Toluene-d8 104% <br /> Instrument ID HP 5972 MS <br /> Analytes reported as ND were not detected or below the Practical Quantitation Llmit <br /> Practical Quantitation Limit= Reporting Limit x Report Limit Multiplication Factor <br /> (pg/L)= micrograms per liter or pa er billion(ppb) <br /> } <br /> I ANALYST r <br /> APPROVED BY <br /> Clary J one Jam s C r lips <br /> IL oratory Director <br />