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' CASTLE ANALYTICAL LABORATORY - PORTERVILLE <br /> Environmental Testing Services 2780 Yowlumne Ave Suite C Phone (559)781-6099 <br />' Porterville, CA 93258 Fax (559) 781-6091 <br /> Advanced GeoEnvironmental Inc Client Project ID Pacific Pride-West Lane Sample Prep Method SW3050 <br />' 937 Shaw Road Reference Number P176 16211 Analysis Method SW6010C <br /> Stockton CA 95215 Sample Description SOIL Prepared 10-21-03 <br /> Attn Tim Cuellar Instrument ID TJA61E Analyzed 10-21-03 <br /> Reported 10-30-03 <br /> QUALITY CONTROL DATA REPORT <br />' SPIKE ID ICP 0213a <br /> Reporting BLANK Spiking Control %R <br /> Limit Result Level Spike Limits <br />' COMPOUNDS mg/kg mg/kg m !k %R <br /> lead 5 0 ND 100 87 8% 80- 120 <br />' Spiking MATRIX MATRIX %R %RPD <br /> Level SPIKE SPIKE DUP Limas <br /> m Ik %R %R <br />' <br /> COMPOUNDS i <br /> Lead 100 640% 720% 1 70- 130 588% <br /> I <br /> The LCS(Laboratory Control Spike)is a control sample of known interferent free matrix that is fortified with representative analytes and <br /> analyzed using the same reagents preparation and analytical methods employed for the samples The LCS%recovery is used for validation <br /> of sample batch results Due to matrix effects the QC limits and recoveries for MS/MSD s are advisory only and are not used to accept or <br /> refect batch results <br /> APPROVED BY <br /> Jams Phi!llps <br /> LaXoratory,Director <br />