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lie <br /> CASTLE ANALYTICAL LABORATORY - PORTERVILLE <br /> Environmental Testing Services 2780 Yowlumne Ave Suite C Phone (559) 781-6099 <br /> Porterville CA 93258 Fax (559)781-6091 <br /> Advanced GeoEnvironmental, Inc Client Project ID Pacific Pride-West Lane Sample Prep Method SW3050 <br /> 937 Shaw Road Reference Number P177/6212 Analysis Method SW6010C <br /> Stockton, CA 95215 Sample Description SOIL Prepared 10-21-03 <br /> Attn Tim Cuellar Instrument ID TJA 61 E Analyzed 10-21-03 <br /> Reported 10-30-03 <br /> QUALITY CONTROL DATA REPORT <br /> SPIKE 1D ICP 0213b <br /> Reporting BLANK Spiking Control %R <br /> Limit Result Level Spike Limits <br /> I mg/kg m Ik m /k %R <br /> COMPOUNDS <br /> Lead 5 0 ND 100 91 5% 80- 120 <br /> ISpiking MATRIX MATRIX %R %RPD <br /> Level SPIKE SPIKE DUP Limits <br /> mg/kg %R %R <br />' COMPOUNDS <br /> Lead 100 800% 813% 70-130 078% <br /> I <br /> I <br />' The LCS(Laboratory Control Spike)is a control sample of known interferent free matrix that is fortified with representative analytes and <br /> analyzed using the same reagents preparation and analytical methods employed for the samples The LCS%recovery is used for validation <br /> of sample batch results Due to matrix effects the QC limsts and recoveries for MSIMSD's are advisory only and are not used to accept or <br />' reject batch results <br />' APPROVED BY <br /> AIZ <br /> James rps <br />' Lad tory Director <br />