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CASTLE ANALYTICAL LABORATORY <br /> Environmental Testing Services 2333 Shuttle Drive, Atwater, CA 95301 Phone (209) 384-2930 <br /> Certificate #2079 Fax (209) 384-1507 <br /> Advanced GeoEnvironmental, Inc Client Pro)ect ID Pacific Pride - West Lane Sampled 8-31-99 <br /> of Northern California Reference Number 2464 Received 9-2-99 <br /> 4005 North Wilson Way Sample Description Sod Extracted 9 2-99 <br /> Stockton, CA 95205 Sample Prep/Analysis Method EPA 5030/8015M, 8020 Analyzed 9 3-99 <br />' Ann Tim Cuellar Lab Numbers 2464-65, 7S, 8S, 9S, 10S Reported 9-15-99 <br /> 1 <br /> I TOTAL PETROLEUM HYDROCARBONS -GASOLINE <br /> WITH STEX DISTINCTION <br /> ANALYTE REPORTING LIMIT SAMPLE ID SAMPLE ID SAMPLE ID SAMPLE ID SAMPLE ID <br /> P3-10 133-20 P3-30 153-35 P4-15 <br />' (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) <br /> MTBE 0 010 39 044 NO 020 13 <br /> BENZENE 00050 NO 0 039 ND NO NO <br /> TOLUENE 00050 052 021 NO 0 025 NO <br /> ETHYL BENZENE 00050 055 0 070 NO NO NO <br /> TOTAL XYLENES 00050 44 0 38 NO 00089 0 048 <br /> IGASOLINE RANGE 1 0 60 1 9 ND NO 42 <br /> HYDROCARBONS <br /> Report Limit Multiplication Factor 10 1 1 1 1 <br /> Report Limit Multiplication Factor MTBE only 50 <br /> Surrogate % Recovery Ne N0.71 1%/PID-70 4% Fal)-63 9%1 PID 64 6% Flp 71 l%!PID 71 7% FID-76 71 PID 76 7% <br /> Instrument ID VAR-GC1 VAR-GC1 VAR-GC1 VAR-GC1 VAR-GC1 <br /> Analytes reported as NO were not detected or below the Practical Quantitation Limit <br /> Practical Quantitation Limit = Reporting Limit x Report Limit Multiplication Factor <br /> ANALYST APPROVED BY / <br /> Clair J Cone WLaboratory <br /> hillips <br /> Director <br />