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. labels (site name, sample location, date, time, and analysis to <br /> be performed) are also noted on the COC form Each person <br /> relinquishing custody of the sample set signs the COC form <br /> indicating the date and time of the transfer to the recipient A <br /> copy of the COC follows the samples or their extracts throughout <br /> the Laboratory to aid the analyst in identifying the samples and <br /> to assure analysis within holding times <br /> Copies of the COC documentation are included with the <br /> laboratory results in Appendix A of this report <br /> MW8 VENTING PROCEDURES <br /> WEGE is using LTT vacuum trucks to pull an estimated 7 - 10 feet <br /> of water vacuum on MW8 , for 2 hours weekly and exhaust directly <br /> to atmosphere This vacuum generates a flow rate of <br /> approximately 64 cfm <br /> COLLECTING SAMPLES <br /> The sample is obtained from a sample port located, prior to the <br /> vacuum pump from a sample port on the flow meter orifice . Sterile <br /> poly tubing was used to attach a one liter tedlar bag, fitted <br /> with a special septum "valve" and tubing bib, to the sample port . <br /> The sample port is on the vaccum side of the pump and therefore a <br /> vacuum greater than the well vacuum must be exerted on the <br /> outside of the tedlar bag to "fill" the bag with the vapor <br /> sample A special vacuum box, in which the tedlar bag is sealed <br /> inside, is used to exert a high vacuum to the exterior of the <br /> bag, thereby pulling a sample into the bag Once the tedlar bag <br /> is filled, its valve is closed and locked and the appropriate <br /> label is placed on the bag <br /> The label shows the date, time, sample ID# and analyses to be run <br /> and the sampler' s initials The tedlar bag samples are then <br /> placed within a cooler, and are hand delivered to WEGE' s <br /> laboratory that same day <br /> The vapor sample is then infected into an FID (Flame Ionizing <br /> Detector) chromatograph and the resulting chromatogram compared <br /> to standard chromatograms of known TPHg (Total Petroleum <br /> Hydrocarbons, gasoline) and BTEX (benzene, toluene, ethylbenzene, <br /> and xylenes) concentrations Selected samples are also analyzed <br /> by second column chromatograph comparison A Photovac 10550 <br /> photo-ionizing gas cnromatograpn was used ro evaivaoe BTEX, LCE, <br /> PCE, and DCE <br /> Carbon dioxide (CO2) concentration is measured from the tedlar <br /> bag samples by connecting a Drager tube and pump to the <br /> inlet/outlet of the tedlar bag CO2 reading in percent is then <br /> obtained and recorded on the chrmoatogram produced from the GC- <br /> FID analysis . <br /> 3 R603 APPEND. D <br />