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10/17/2000 09:00 2094683433 <br /> FIFTI-I FLOOR PACS 08 <br /> 1V�'11"171"d VERUTCATJQN LAB o A TORY AXALYSX3 <br /> ANK TANK TPH-G TPH-D ]rTX doaW oxvcrnwrt$ <br /> CONTENTS $DIS 8415 8020 CL HC TOTAL MTBE <i1 eE, AUTALS PCB <br /> 8260 $260 8260 8010 LEAD 8070 Em 1PE IC8,270 <br /> 8244 74�0 wAESS <br /> 8260 7421 8269 TAME)am or 8080 <br /> AA <br /> LEADED OAS X X <br /> X X <br /> UNL GAS X X <br /> x <br /> DIF-SEL x x <br /> KEROSENE x x x <br /> UNK FUEL x x x x <br /> x <br /> PROD OIL x x x <br /> CHLOR_ <br /> i <br /> S4LVBNY'S X X x <br /> NONCHLOR <br /> SOLVENTS X x x <br /> 'BASTE, <br /> USED 071. x x x x <br /> X X X <br /> AU atmlyai,methods are dee designated EPA metbnda desenbcd m EPA SW 844, 'Third Edition Those methods rto2(aurid !n SW <br /> 846 are;pacifically noted below Refer to the "SWRCB LU>=T Fleld Manual",Appendix D (B), Table 3-3 on page A2()fax <br /> ln=tun detection I mics for motor vehicle ftwl(Sasollne and diesel} Refer to`Tri>aGegioaai Hoard�at�Itecamtricndaaions far <br /> utial&rraltsaaoa and Invtstigatiarf of UST's" for rise waste asci motor osl WAnixnj=detectlan amts. <br /> l ktv"Wa L' that rem8lu b@40w the MCL, STLC or AUdwoble Limit or thr cunt~arah=t in quesdan will be accepted, <br /> bowrrrsr lobwatery aball utiliize the mast cmwrvahve xnxtTau& <br /> LABORATORY ANALYSES TERM1NoLoGY <br /> TPH-D Toil Parpleum Hydrocarbon, 02Sp11rie; GCIF3D <br /> 17H-D Torsi Petroleum H (5030)SUSS rood or GCJMS 8260 <br /> BTX&H ydrocarbon. Diesel,GVFW(3350), 8013 mod of GC/MS 8260 <br /> CL HC Bcnz�• Toluene:. Xylent&Ethyl$enzexie, GCfPM 8020 or GCJM3 8260 <br /> Chlorinated Hydrocarbon, GCIMD Solo, GCIMS 8240 or SM <br /> TOT'S'LEAD TOW ltrad, AA 7420, AA 7421 or JCP AES 6010 <br /> OXYGENATES MTBE.,ETBE.TAME.DIPE,&TBA <br /> GC/MS 92m(For MTS&screen only you may use 8070) <br /> METALS ICAIs or AA lticiticuvcly C <br /> otipied Plasrrta Atomic Emissian 5peetromet>•y 6010 or Atomic Absorption Spectrometry 7000 <br /> PCB N19ta4- C*drottrria,Chromium III and V1,Lead,Zinc and Nickel. <br /> Polychlorinated Blyhergls. GCIMS x270 or 808o <br /> GC-FID Gas Chromamimphy, Flatus J4Derlrsttl0n DKreetron <br /> Method 3050 Acid digestion <br /> Meibod 3540 Soxhltt sample preparuion <br /> Method 3550 SOtiiMOtt tatityie Preparation, extract,on method <br /> QMH 5030 Purge=d trap sar�z p:rep&m%-;On <br /> QC Qtiailty Assurance/Qtiailty Control <br /> lyvLes s o avoia false positive detection of benzene,benzene-thee solvents are to be used FUsed capillarycolumns are preferred m paged <br /> c0luinw,a packed column may be used as a"first cut'with 'd;M'samples or once the hydrocaabons Marr lfeeet chiiracrCr[zed orad p P� <br /> QAtQC is fajiAwed <br /> For drinking water sources, EPA recommends that clic 500 scrips for volatile organic should be used in prcfaewc to the Wo series becau ,the <br /> detCetlon ltinit3 etre lcwCr and the QA/QC is better, 5axnpies exhibivn$any 1eve:1 of hcav} mewl conjam,"Itlon may require further smillyss,- <br /> ed <br /> PHS-EHD recocsumnds holding those samples until disposal is nidic. <br /> EH 23 046 (RevlSec105r09100) Past 8 <br />