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R603 UPDATE-12 12/22/92 <br /> 40 Then the syringe is filled, the sample valve closed, and forceps <br /> are clamp onto the soft polytubing to create an air tight seal <br /> before removing the syringe from the sample port Once the 60 cc <br /> syringe is removed with the clamped polytubing attached, the <br /> plunger is pushed into the syringe to create pressure within the <br /> syringe and released to allow the collected vapors to reach <br /> equilibrium A small dedicated needle attached to a dedicated 1 <br /> cc syringe is then inserted into the 60 cc syringe via the soft <br /> tubing for obtaining the sample to be injected into the PID-GC <br /> Again the 1cc syringe is purged numerous times before filling it <br /> with the sample All but 0 5 cc of the sample is ejected into <br /> the air before infecting the remaining 0 5 cc syringe sample into <br /> the GC-PID (the calibrant injection is 0 5 cc) Once the <br /> chromatogram is recorded an instrument blank is run prior to the <br /> next sample . The instrument blank indicates if residual peaks <br /> are being carried onto the next analysis <br /> While the GC-PID analysis is running for a particular sample (15 <br /> minutes per sample run) , vacuum influent readings are obtained <br /> from the wells by attaching a manometer calibrated in mm water to <br /> sample ports at the well heads These readings show the mm water <br /> pressure or vacuum that is being created at each well <br /> Occasionally the 10550 PID-GC is not available for field <br /> determination of the influent and effluent streams . Tedlar bag <br /> samples are then obtained and brought back to the WEGE portable <br /> laboratory for analysis using an FID-GC, see Appendix C - Field <br /> Notes . <br /> VAPOR RECOVERY OPERATIONS AND RESULTS <br /> As stated in earlier reports, soil contamination exists from <br /> beneath the tank excavation to the top of the ground water, see <br /> Fence Diagram Figure 6 Overexcavation during the initial tank <br /> removal, removed contaminated soil to the 25 foot depth. Before <br /> replacing the new double contained fiberglass tanks and <br /> dispensing system, 4 inch and 6 inch SCH 40 PVC 0 . 02 inch slotted <br /> pipes were placed vertically at the north corner and west corner <br /> of the excavation respectively and manifolded via underground to <br /> the treatment compound with SCH 40 2 inch and 4 inch PVC pipe. <br /> These pipes along with monitor wells MW1, MW2 , MW3 and MW10 are <br /> used for vapor extraction for soil and ground water remediation <br /> On October 10, 1991 the vapor extraction system operated six <br /> L L 1_ s..L i-.-, l.. �.�.. r7 —rr.-+o r�� A f-iii r+t i ^" r-%f t}1P <br /> 11UL1J' s, l o clie ck 1.h.e aLLL.V .rye 111A 1..Cd0 W l i s aiiu tdci� —. —ti.4 a44—Al <br /> REMOX unit, using monitor wells MW1, MW10, and the excavation <br /> wells . The system was restarted on October 17, 1991 and initial <br /> inspection and operation of the system occurred The unit <br /> operated until November 5, 1991, when it was shut down to replace <br /> a worn bear a ag . The system was rest-ar ted on November 20, 1991 <br /> and operated until December 24, 1991 . On this date someone <br /> turned off the main breaker that services the treatment compound <br /> This breaker box has since been locked. The unit was restarted <br /> on January 3 , 1992 and operated until July 20, 1992, with <br /> PAGE 7 <br />