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i <br /> North State Environmental Laboratory CA FLAP# 3753 <br /> 90 South Spruce Avenue, Suite V • South San Francisco, CA 94080 • (650) 266-4563 • FAX (650) 266-4560 <br /> CERTIFICATE OF ANALYSIS <br /> Job Number 00-0268 Date Sampled 02/25/2000 <br /> Client Wickland Properties Date Analyzed 02/28/2000 <br /> Pro3ect R603-Confirmation Date Reported 03/10/2000 <br /> Volatile Organics by GC/MS Method 8260 <br /> Quality Control/Quality Assurance Summary <br /> Laboratory Number 00-0268 MS/MSD RPD <br /> Client ID Blank Recovery <br /> Matrzx SOIL SOIL <br /> Aralyte Results %Recoveries <br /> ug/Kg <br /> Ethanol ND<500 <br /> Methyl-t-Butyl Ether I\D<50 <br /> Di-isopropyl Ether ND<5 <br /> tertiary 5utyl Alcohol hril<250 <br /> Ethyl-t-Butyl Ether ND<5 <br /> t-Amyl Nethyl Ether ND<5 <br /> 1,1-Dzchloroethene ND<5 114 6 <br /> nzeneND<5 130 4 <br /> cnloroethene hD<5 101 7 <br /> toluene ND<5 101 2 <br /> Chlorobe-izene hTD<5 114 4 <br /> SUR-Dibromofluoromethane 79% Rec 101/85 17 <br /> SUR-Toluene-d8 95% Rec 101/101 0 <br /> SUR-4-Bromofluorobenzene 117% Rec 100/98 2 <br /> Re7ilwed d A pr d <br /> r <br /> I <br /> John A Murphy <br /> Laboratory Director <br /> Page 3 Of 3 <br />