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v I ` F WORK ORDER: 9709248 QUALITY CONTROL. REPORT PAGE QR-3 ANALYSIS: Gasoline Oxygenates MATRIX: Water! MATRIX SPIKE DUPLICATES ----------------------------------------------------------•---........................._............------...---............. SAMPLE TYPE: Spiked Sample Duplicate LAB ID: MR09248-04D INSTR RUN: GCMS121970925000000/16/14 INSTRUMENT: HP mass spec for Volatiles PREPARED: BATCH ID: MS12WO92697 UNITS: ug/L ANALYZED: 09/26/97 DILUTION: 1.00 METHOD: EPA 8260 REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) 1,2-DCE-d4 (surr) 115 114 100 115 70 130 Toluene-d8 (surr) 99.8 103 100 99.8 70 130 Bromofluorobenzene (surr) 102 105 100 102 70 130 Methy-t•butyl ether (MTBE) 121 126 5 4.05 25 Ethyl-t•butyl ether (ETBE) 135 133 5 1.49 25 t-Amylmethyl ether (TAME) 124 129 5 3.95 25 t-Butanol (TBA) ND ND 100 0 Di-isopropyl ether (DIPE) ND ND 5 0 SAMPLE SURROGATES ................•----------•--...---------------..............------....--------------------------------..................... SAMPLE TYPE: Sample-Client LAB ID: 9709248-01D INSTR RUN: GCMS121970925000000/10/ INSTRUMENT: HP mass spec for Volatiles PREPARED: BATCH ID: MS12WO92697 UNITS: ug/L ANALYZED: 09/26/97 DILUTION: 1.00 METHOD: EPA 8260 REF REPORTING SPIKE RECOVERY REG LIMITS (X) RPD ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) "-' 1.2-DCE d4 (surr) 115 100 115 70 130 Toluene•d8 (surr) 97.8 100 97.8 70 130 Bromofluorobenzene (surr) 104 100 104 70 130 .........................................................•-•----•-------•----...................•••........•-----......-••--- ...............•---------------...........---------..............--------------..............................----............ SAMPLE TYPE: Sample-Client LAB ID: 9709248-02D INSTR RUN: GCMS121970925000000/11/ INSTRUMENT: HP mass spec for Volatiles PREPARED: BATCH ID: MS12W092697 UNITS: ug/L ANALYZED: 09/26/97 DILUTION: 1.00 METHOD: EPA 8260 REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) 1,2-DCE-d4 (surr) 109 100 109 70 130 Toluene-dB (surr) 103 100 103 70 130 Bromofluorobenzene (surr) 104 100 104 70 130 -•------••---•..........................................•--•-----........--- ................................................ ----------------------------------------------------------------------------------------------------------------------------- SAMPLE TYPE: Sample-Client LAB ID: 9709248-03D INSTR RUN: GCMS121970925000000/12/ INSTRUMENT: HP mass spec for Volatiles PREPARED: BATCH ID: MS12WO92697 UNITS: ug/L ANALYZED: 09/26/97 DILUTION: 1.00 METHOD: EPA 8260 REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X). 1.2-DCE-d4 (surr) 113 100 113 70 130 Toluene-d8 (surr) 98.4 100 98.4 70 130 Bromofluorobenzene (surr) 98.1 100 98.1 70 130 ..............•----------....---•--------........_...----.........------------...................------...----........------. SAMPLE TYPE: Sample-Client LAB ID: 9709248-04D INSTR RUN: GCMS121970925000000/13/ INSTRUMENT: HP mass spec for Volatiles PREPARED: BATCH ID: NS12WO92697 UNITS: ug/L ANALYZED: 09/26/97 DILUTION: 1.00 METHOD: EPA 8260 REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) 1.2-DCE•d4 (surr) 110 100 110 70 130 Toluene-d8 (surr) 103 100 103 70 130 Bromofluorobenzene (surr) 102 100 102 70 130 i ....................................................... .....................................................................