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7. q:11 A L I T Y ..A' S.'S- b..k A N C E WE N.q.O:..g::... :.. :. R-1.F E R E NCE s A N: D ..,N.0•.7.E ........ : Re ....... '.... orE:Dflte-..:03l:1:ITF�a4`�•:: ............... r REPORT COMMENTS 1) All pages of this report are integral parts of the analytical data_ Therefore, this report should be reproduced only in its entirety. K 2) Boit, sediment and sludge sample results are reported on a "dry weight" basis except when analyzed for landfill disposat or incineration parameters. All other solid matrix samples are reported on an "as 'Zi received" basis unless noted differently. 3) Reporting limits are adjusted for sample size used, dilutions and moisture content if applicable. 4) The test results for the noted anatyticat. method(s) meet the requirements of NELAC. Lab Cert- ID# 100201 r` 5) Actbrding to 40CFR Part 136.3, pH, Chlorine Residual and Dissolved oxygen analyses are to be performed immediately after aqueous sample collection_ When these parameters are not indicated a4 field (e.g. pH Field) they were not analyzed immediately, but as soon as passible an laboratory receipt. Glossary of flags, qualifiers and abbreviations (any number of which may appear in the report) -'' Inorganic Qualifiers (9-Colum) U Analyte was not detected at or above the stated limit. < Not detected at or above the reporting limit. i Result is less then the kL, but greater than or equal to the method detection limit. B Result is less than the CRDL/RL, but greater than or equal to the IDLIMDL. S Result was determined by the Method of Standard Additions. F AFCEE: Result is less than the RL, but greater than or equal to the method detection limit. Inorganic Flags (FLag Column) F.T ICV,CCV,ICB,CCB,ISA,isB,GRI,CRA,MRL: instrument related QC exceed the upper or lower '� '• F -3 control limits. LC5, LCD, MD: Batch QC exceeds the upper or loner control limits_ + MSA correlation coefficient is tens than 0.995. 4 HS, HSD: The analyte present in the original sampte is 4 times greater than the matrix spike concentration; therefore, control limits are not applicable. '4 E SD: serial- dilution exceeds the control limits. H MB, Eat, EB2, EB3: Batch vC is greater than reporting omit or had a negative instrument reading lower than the absolute value of the reporting limit. N MS, MSD: Spike recovery exceeds the upper or tower control limits. W AS(GFAA) Post-digestion spike was outside 55-115% control Limits, Organic Quetiflers (u - Column) U Analyte was not detected at or above the stated Limit. ND Compound not detected. i Result is an estimated value below the reporting limit or a tentatively - 4 if identified compound (TIC). ; 4 Result was qualitatively confirmed, but not quantified. C Pesticide identification was confirmed by GUMS. Y The chromatographic response resembles a typical fuel pattern_ __ t The chromatographic response does not resemble a typical fuel pattern. ?# E Result exceeded calibration range, serandery dilution required- •. : F AFCEE:Result is an estimated value below the reporting limit or a tentatively identified compound (TiC) Organic Flags (Flago Column) 8 MB: Batch QC is greater then reporting limit. 01 (C6, LCD, ELC, ELD, CV, MS, MSD, surrogate! Batch QC exceeds the upper or lower control limits_ E,r E81, E92, E93, MLE: Batch AC is greater than reporting limit A Concentration exceeds the in8trument calibration range a Concentration is below the method Reporting Limit (RL) B Compound was found in the blank and sample. D Surrogate or matrix spike recoveries were not obtained because the extract was diluted for analysis; also compounds analyzed at a dilution will be flagged with a D. H Alternate peak selection upon analytical review I indicates the presence of an interfpnce, recovery is not calculated. c'?i M Manually integrated compound. P The tower of the two values is reported when the % difference between the results of two GC columns is Page 21 „r�