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t <br /> i <br /> Lim, � <br /> e <br /> Quality Control Results <br /> t Client: San Joaquin Company Inc <br /> Job Number: 720-1181-1 <br /> rl Matrix Spike/ Method: 8260B <br /> Matrix Spike.Duplicate Recovery Report-Batch: 720-3681 Preparation: 50308 <br /> .I <br /> MS Lab Sample ID: 720-1181-5 Analysis Batch: 720-3681 Instrument ID: Saturn 2100 <br /> Client Matrix: Water Prep Batch: NIA Lab File ID: d:Idata1200512112270517: <br /> Dilution: 1.0 Initial WeightlVolume: 10 mL <br /> Date Analyzed: 12/28/2005 0348 Final Weight/Volume: 10 mL <br /> Date Prepared: 12/28/2005 0348 <br /> MSD Lab Sample ID: 720-1181-5 Analysis Batch, 720-3681 Instrument ID: Saturn 2100 <br /> E t: Client Matrix: Water Prep Batch: NIA Lab File ID: d:Idata12005121122705172( <br /> Dilution: 1.0 initial WeightfVolume: 10 mL <br /> Date Analyzed: 12/28/2005 0415 Final WeightNolume: 10 mL <br /> I Date Prepared: 12/28/2005 0415 <br /> % Rec. <br /> Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual <br /> Benzene 88 91 V 69-129 3 20 <br /> MTBE 108 77 65-165 12 20 <br /> Toluene 88 91 70-130 3 20 <br /> U Surrogate MS%Rec MSD% Rec Acceptance Limits <br />{ Toluene-d8 99 100 77- 121 <br /> 1,2-Dichloroethane-d4 88 81 73- 130 <br /> k <br /> i <br /> II <br /> 1. <br /> �rJ•i <br /> �r <br /> Y*: <br /> Calculations are performed before rounding to avoid round-off errors in calculated results. <br /> l STL San Francisco Page 44 of 56 <br /> r <br />