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I <br /> GeoAnalytical Laboratories, Inc. <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone (209)572-0900 Fax (209)572-0916 <br /> CERTIFICATE OF ANALYSIS <br /> Qeport# M178-14 Date: 7/03/01 <br /> Date Rec'd: 6/27/01 <br /> M.J. Kloberdanz &Associates Project: Old Shell Sation-Escalon/Quarterly Date Started: 7/02/01 <br /> P.O.Box 576981 Date Completed: 7/03/01 <br /> Modesto CA 95357 PO# <br /> Date Sampled: 6/27/01 <br /> Time: <br /> Sampler : R Azevedo(Geo) <br /> Sample ID: MW-2 - <br /> Lab ID: M306369 <br /> Method RL Analyte Results Units <br /> 8260B 3.0 Benzene 29 ug/L <br /> 3.0 Toluene 160 <br /> 3.0 Ethyl Benzene 29 <br /> 6.0 Total Xylenes 93 <br /> 10 Methyl tent-butyl ether (MTBE) 10 <br /> 400 Ethanol ND <br /> 200 tert-Butanol ND <br /> 10 di-Isopropyl ether (DIPE) ND <br /> 10 Ethyl tert-butyl ether (ETRE) ND <br /> 10 tert-Amyl methyl ether (TAME) ND <br /> 10 Ethylene dibromide (EDB) ND <br /> 5 1,2-Dichloroethane (1,2-DCA) ND <br /> h <br /> Surrogate Amnt Spiked Amnt Recovered %Recovery QC Limit% <br /> 1,2-Dichloroethane-d4 50 51.9 103.8 72-132 <br /> 2-Bromo-l-chloropropane 50 29.1 58.2 71-134 <br /> 4-Bromofluorobenzene 50 48.2 96.4 74-132 <br /> I � <br /> Mario D'Onofrio Donna Keller <br /> Chemist Certification # 1157 Laboratory Director <br />