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14.1 Alpha Analytical, Inc law 255 Glendale Ave. -Suite 21 •Sparks,Nevada 89431-5778 (775)355-1044•(775)355-0406 FAX • 1-800-283-1183 Date: OC SL1nuna'yReport Work Order: 01-Au¢-03 03072125 _ Method Blank Type MBLK Test Cade: EPA Method 300.0/9056 File ID: Batch ID:8218A Analysis Dale: 07/21/2003 17:05 Sample ID: MBLK_8218A Units: mg1L Run ID:IC 1 030721A Prep Date: 071211203 0 Analyte Result PQL SpkVal SpkReNal %REC Lowl-imit HighLimit RPD Ref Val %RPD Qua[ Nitrate(NO3)-N NO 0.25 Laboratory Control Spike Type LCS Test Code: EPA Method 300.0/9056 File ID: Batch ID:8218A Analysis Date: 07/21/2003 17:23 ` Sample ID: LCS_821 SA Units:mg/L Run 10:IC_1_030721A Prep Date: 07/21/2 0 03 Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPD Ref Val %RPD Qual Nitrate(NO3)-N 2.01 0.25 2 100 90 110 r Sample Matrix Spike Type MS Test Code: EPA Method 300.019056 File ID: Batch 10:8218A Analysis Date: 07/2112003 19:07 Sample 10: 03072124-04AMS Units: mglL Run ID:IC_t_030721A Prep Date: 07/2112003 Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPD Ref Vat %RPD Qual Nitrate(NO3)-N 5.24 0.25 2 3.5 87 80 120 Sample Matrix Spike Duplicate Type MSD Test Code: EPA Method 300.0 1 9056 ` File ID: Batch ID:8218A Analysis Dale: 07121/2003 19:25 Sample ID: 03072124-04AMSD Units:mg/L Run ID:IC_t_030721A Prep Date: 07/21/1003 Analyte Result POL SpkVal SpkRefVal %REC Lowlimit HighLimit RPD Ref Val %RPD Qual Nitrate(NO3)-N 5.23 0.25 2 3.5 86 80 120 5.239 0.808 Comments: NO-Not Detected at the Reporting Limit. D-if the spiked value is<25%of the reference value,recovery should not be calculated. S-Spike Recovery outside accepted recovery limits. M-Spike Recovery outside accepted recovery limits due to matrix. ` B-Analyte detected in the associated Method Blank. r r r fr s. r